[17O]-labeled bis[2-(hydroxymethyl)phenyl] diselenide

Base Information

• Chemical Name: [17O]-labeled bis[2-(hydroxymethyl)phenyl] diselenide
• CAS No.: 697792-93-1
• Molecular Formula: C₁₄H₁₄O₂Se₂
• Molecular Weight: 374.185
• Mol file: 697792-93-1.mol

Synonyms:[17O]-labeled bis[2-(hydroxymethyl)phenyl] diselenide

Chemical Property of [17O]-labeled bis[2-(hydroxymethyl)phenyl] diselenide

Chemical Property:

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Technology Process of [17O]-labeled bis[2-(hydroxymethyl)phenyl] diselenide

There total 1 articles about [17O]-labeled bis[2-(hydroxymethyl)phenyl] diselenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

[17O]-labeled bis(2-formylphenyl) diselenide (697792-86-2) → [17O]-labeled bis[2-(hydroxymethyl)phenyl] diselenide (697792-93-1)

Guidance literature:

With sodium tetrahydroborate; In methanol;

DOI:10.1021/ja049690n

Reference yield:

[17O]-labeled bis[2-(hydroxymethyl)phenyl] diselenide (697792-93-1) → [17O]-labeled 2-(hydroxymethyl)benzeneselenenyl chloride

Guidance literature:

With sulfuryl dichloride; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1021/ja049690n

Reference yield:

[17O]-labeled bis[2-(hydroxymethyl)phenyl] diselenide (697792-93-1) → [17O]-labeled 2-(hydroxymethyl)benzeneselenenyl bromide

Guidance literature:

With bromine; In dichloromethane; for 0.25h;

DOI:10.1021/ja049690n

upstream raw materials:

[17O]-labeled bis(2-formylphenyl) diselenide