(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*Mn(CO)3TeC₆H₄NH^(1-)=(C₆H₅)3PNP(C₆H₅)3Mn(CO)3TeC₆H₄NH

Base Information

• Chemical Name: (C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*Mn(CO)3TeC₆H₄NH^(1-)=(C₆H₅)3PNP(C₆H₅)3Mn(CO)3TeC₆H₄NH
• CAS No.: 352531-72-7
• Molecular Formula: C₉H₅MnNO₃Te*C₃₆H₃₀NP₂
• Molecular Weight: 896.27

Synonyms:(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*Mn(CO)3TeC₆H₄NH^(1-)=(C₆H₅)3PNP(C₆H₅)3Mn(CO)3TeC₆H₄NH

Chemical Property of (C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*Mn(CO)3TeC₆H₄NH^(1-)=(C₆H₅)3PNP(C₆H₅)3Mn(CO)3TeC₆H₄NH

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Technology Process of (C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*Mn(CO)3TeC₆H₄NH^(1-)=(C₆H₅)3PNP(C₆H₅)3Mn(CO)3TeC₆H₄NH

There total 1 articles about (C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*Mn(CO)3TeC₆H₄NH^(1-)=(C₆H₅)3PNP(C₆H₅)3Mn(CO)3TeC₆H₄NH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

bis(triphenylphosphineiminium) pentacarbonylmanganate(1-) (52542-59-3,192520-17-5) + 2,2’-ditellanediyldianiline (72695-32-0) → (C6H5)3PNP(C6H5)3(1+)*Mn(CO)3TeC6H4NH(1-)=(C6H5)3PNP(C6H5)3Mn(CO)3TeC6H4NH (352531-72-7)

Guidance literature:

With O₂; In tetrahydrofuran; byproducts: CO; Mn-complex and ligand were dissolved in THF, stirred at ambient temp. under inert atm., O2 was bubbled through soln.; filtered, hexane was added, washed with hexane, recrystd. from THF-hexane; elem. anal.;

DOI:10.1021/ic000795a

Reference yield:

(C6H5)3PNP(C6H5)3(1+)*Mn(CO)3TeC6H4NH(1-)=(C6H5)3PNP(C6H5)3Mn(CO)3TeC6H4NH (352531-72-7) + Benzene-1,2-dithiol (17534-15-5) → N(P(C6H5)3)2(1+)*Mn(CO)3(C6H4S2)(1-) = [N(P(C6H5)3)2][Mn(CO)3(C6H4S2)] (243974-14-3)

Guidance literature:

In tetrahydrofuran; to stirred soln. of Mn-complex in THF was added ligand under N2 at room temp., stirred for 5 min; monitored by IR;

DOI:10.1021/ic000795a

Reference yield:

ortho-mercaptophenol (1121-24-0) + (C6H5)3PNP(C6H5)3(1+)*Mn(CO)3TeC6H4NH(1-)=(C6H5)3PNP(C6H5)3Mn(CO)3TeC6H4NH (352531-72-7) → (C6H5)3PNP(C6H5)3(1+)*Mn(CO)3SC6H4O(1-)=(C6H5)3PNP(C6H5)3Mn(CO)3SC6H4O

Guidance literature:

In tetrahydrofuran; to stirred soln. of Mn-complex in THF was added ligand under N2 at room temp., stirred for 5 min; monitored by IR;

DOI:10.1021/ic000795a

upstream raw materials:

bis(triphenylphosphineiminium) pentacarbonylmanganate^(1-)

2,2’-ditellanediyldianiline

Downstream raw materials:

N(P(C₆H₅)3)2⁽¹⁺⁾*Mn(CO)3(C₆H₄S₂)^(1-) = [N(P(C₆H₅)3)2][Mn(CO)3(C₆H₄S₂)]

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