C₄₈H₅₄O₄Si₂

Base Information

Chemical Name:C₄₈H₅₄O₄Si₂
CAS No.:1304037-72-6
Molecular Formula:C₄₈H₅₄O₄Si₂
Molecular Weight:751.125
Hs Code.:

C<sub>48</sub>H<sub>54</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₄₈H₅₄O₄Si₂

Suppliers and Price of C₄₈H₅₄O₄Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₈H₅₄O₄Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₈H₅₄O₄Si₂

There total 4 articles about C₄₈H₅₄O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1304037-71-5
C₄₈H₆₂O₄Si₂

: 1304037-72-6
C₄₈H₅₄O₄Si₂

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 3h; Molecular sieve; Inert atmosphere;
DOI:10.1055/s-0030-1258385

Reference yield:

: 1019742-69-8
diethyl 2-((triisopropylsilyl)ethynyl)-5-((trimethylsilyl)ethynyl)terephthalate

: 1304037-72-6
C₄₈H₅₄O₄Si₂

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / tetrahydrofuran / 8 h / 20 °C / Inert atmosphere

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 4 h / Inert atmosphere

3: diisobutylaluminium hydride / tetrahydrofuran; hexane / 0 - 20 °C

4: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Molecular sieve; Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisobutylaluminium hydride; potassium carbonate; triethylamine; pyridinium chlorochromate; In tetrahydrofuran; hexane; dichloromethane; 2: Sonogashira cross-coupling;
DOI:10.1055/s-0030-1258385

Reference yield:

: 1304037-70-4
C₅₂H₆₂O₈Si₂

: 1304037-72-6
C₄₈H₅₄O₄Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 0 - 20 °C

2: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Molecular sieve; Inert atmosphere

With diisobutylaluminium hydride; pyridinium chlorochromate; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1055/s-0030-1258385