2-[(1-benzyl-5-methyl-3-oxido-1H-imidazol-4-yl)carbonyl]-N-methylhydrazinecarbothioamide

Base Information

• Chemical Name: 2-[(1-benzyl-5-methyl-3-oxido-1H-imidazol-4-yl)carbonyl]-N-methylhydrazinecarbothioamide
• CAS No.: 1349129-84-5
• Molecular Formula: C₁₄H₁₇N₅O₂S
• Molecular Weight: 319.387

Synonyms:2-[(1-benzyl-5-methyl-3-oxido-1H-imidazol-4-yl)carbonyl]-N-methylhydrazinecarbothioamide

Chemical Property of 2-[(1-benzyl-5-methyl-3-oxido-1H-imidazol-4-yl)carbonyl]-N-methylhydrazinecarbothioamide

Chemical Property:

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Technology Process of 2-[(1-benzyl-5-methyl-3-oxido-1H-imidazol-4-yl)carbonyl]-N-methylhydrazinecarbothioamide

There total 2 articles about 2-[(1-benzyl-5-methyl-3-oxido-1H-imidazol-4-yl)carbonyl]-N-methylhydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-benzyl-5-methyl-1H-imidazole-4-carbohydrazide 3-oxide (1349129-34-5) + methyl thioisocyanate (556-61-6) → 2-[(1-benzyl-5-methyl-3-oxido-1H-imidazol-4-yl)carbonyl]-N-methylhydrazinecarbothioamide (1349129-84-5)

Guidance literature:

In ethanol; for 2h; Reflux;

DOI:10.1002/hlca.201100292

Reference yield:

benzylamine (100-46-9) → 2-[(1-benzyl-5-methyl-3-oxido-1H-imidazol-4-yl)carbonyl]-N-methylhydrazinecarbothioamide (1349129-84-5)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid

2: hydrazine hydrate / methanol

3: ethanol / 2 h / Reflux

With hydrazine hydrate; acetic acid; In methanol; ethanol;

DOI:10.1002/hlca.201100470

Reference yield: 72.0%

2-[(1-benzyl-5-methyl-3-oxido-1H-imidazol-4-yl)carbonyl]-N-methylhydrazinecarbothioamide (1349129-84-5) → 5-(1-benzyl-5-methyl-3-oxido-1H-imidazol-4-yl)-2,4-dihydro-4-methyl-3H-1,2,4-triazole-3-thione (1349129-87-8)

Guidance literature:

With sodium hydroxide; In water; for 2h; Reflux;

DOI:10.1002/hlca.201100292

upstream raw materials:

1-benzyl-5-methyl-1H-imidazole-4-carbohydrazide 3-oxide

methyl thioisocyanate

benzylamine

Downstream raw materials:

5-(1-benzyl-5-methyl-3-oxido-1H-imidazol-4-yl)-2,4-dihydro-4-methyl-3H-1,2,4-triazole-3-thione

5-(1-benzyl-5-methyl-3-oxido-1H-imidazol-4-yl)-N-methyl-1,3,4-thiadiazol-2-amine

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