Technology Process of C44H60N6O16
There total 5 articles about C44H60N6O16 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylphosphite copper(I) iodide complex;
In
methanol; chloroform;
at 100 ℃;
for 3h;
Reagent/catalyst;
Temperature;
Time;
Sealed tube;
Microwave irradiation;
DOI:10.1021/bc500047r
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen azide; triphenylphosphine; di-isopropyl azodicarboxylate / toluene; N,N-dimethyl-formamide / 0 - 20 °C
2: triethylphosphite copper(I) iodide complex / methanol; chloroform / 3 h / 100 °C / Sealed tube; Microwave irradiation
With
hydrogen azide; triethylphosphite copper(I) iodide complex; di-isopropyl azodicarboxylate; triphenylphosphine;
In
methanol; chloroform; N,N-dimethyl-formamide; toluene;
2: |Huisgen Cycloaddition;
DOI:10.1021/bc500047r
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / toluene; N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere
2: trichlorophosphate / 12 h / 0 - 40 °C / Inert atmosphere
3: piperidine / acetonitrile / 12 h / 20 °C / Inert atmosphere
4: triethylphosphite copper(I) iodide complex / methanol; chloroform / 3 h / 100 °C / Sealed tube; Microwave irradiation
With
piperidine; triethylphosphite copper(I) iodide complex; sodium hydride; trichlorophosphate;
In
methanol; chloroform; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil;
2: |Vilsmeier-Haack Formylation / 3: |Knoevenagel Condensation / 4: |Huisgen Cycloaddition;
DOI:10.1021/bc500047r
