C₂₄H₂₁ClFN₃O₇

Base Information

Chemical Name:C₂₄H₂₁ClFN₃O₇
CAS No.:1445389-55-8
Molecular Formula:C₂₄H₂₁ClFN₃O₇
Molecular Weight:517.898
Hs Code.:

C<sub>24</sub>H<sub>21</sub>ClFN<sub>3</sub>O<sub>7</sub>

Synonyms:C₂₄H₂₁ClFN₃O₇

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Chemical Property of C₂₄H₂₁ClFN₃O₇

Chemical Property:

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Technology Process of C₂₄H₂₁ClFN₃O₇

There total 15 articles about C₂₄H₂₁ClFN₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.9%

: 1445389-50-3
C₂₄H₂₀ClFN₂O₇

: 1445389-55-8
C₂₄H₂₁ClFN₃O₇

Guidance literature:: C₂₄H₂₀ClFN₂O₇; With dmap; Triphenylsilyl chloride; triethylamine; In acetonitrile; at 20 ℃; for 3h;

With hydroxylamine hydrochloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 2h;

Reference yield:

: 56287-17-3,69123-94-0,784-71-4
2'-deoxy-2'-fluorouridine

: 1445389-55-8
C₂₄H₂₁ClFN₃O₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: pyridine / 20 °C

2.1: silver nitrate; 2,4,6-trimethyl-pyridine / dichloromethane / 20 °C

2.2: 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

4.1: pyridine; Dess-Martin periodane / dichloromethane / 4 h / 0 - 20 °C

4.2: 20 °C

5.1: pyridine / dichloromethane / 0.83 h / -35 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

7.1: lithium chloride / 2 h

8.1: sodium hydroxide / tetrahydrofuran; water / 1 h / 20 °C

9.1: formic acid / 20 °C

10.1: pyridine / acetonitrile / 2.5 h / 0 - 20 °C

11.1: Triphenylsilyl chloride; dmap; triethylamine / acetonitrile / 3 h / 20 °C

11.2: 2 h / 20 °C

With pyridine; 2,4,6-trimethyl-pyridine; dmap; formic acid; Triphenylsilyl chloride; tetrabutyl ammonium fluoride; sodium hydride; Dess-Martin periodane; silver nitrate; triethylamine; lithium chloride; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: C₂₅H₂₉FN₂O₅Si

: 1445389-55-8
C₂₄H₂₁ClFN₃O₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: silver nitrate; 2,4,6-trimethyl-pyridine / dichloromethane / 20 °C

1.2: 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

3.1: pyridine; Dess-Martin periodane / dichloromethane / 4 h / 0 - 20 °C

3.2: 20 °C

4.1: pyridine / dichloromethane / 0.83 h / -35 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

6.1: lithium chloride / 2 h

7.1: sodium hydroxide / tetrahydrofuran; water / 1 h / 20 °C

8.1: formic acid / 20 °C

9.1: pyridine / acetonitrile / 2.5 h / 0 - 20 °C

10.1: Triphenylsilyl chloride; dmap; triethylamine / acetonitrile / 3 h / 20 °C

10.2: 2 h / 20 °C

With pyridine; 2,4,6-trimethyl-pyridine; dmap; formic acid; Triphenylsilyl chloride; tetrabutyl ammonium fluoride; sodium hydride; Dess-Martin periodane; silver nitrate; triethylamine; lithium chloride; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;