N-((1,1-dimethyl-1H-inden-2-yl)methyl)-4-methyl-N-phenylbenzenesulfonamide

Base Information

Chemical Name:N-((1,1-dimethyl-1H-inden-2-yl)methyl)-4-methyl-N-phenylbenzenesulfonamide
CAS No.:1499076-71-9
Molecular Formula:C₂₅H₂₅NO₂S
Molecular Weight:403.545
Hs Code.:

Synonyms:N-((1,1-dimethyl-1H-inden-2-yl)methyl)-4-methyl-N-phenylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((1,1-dimethyl-1H-inden-2-yl)methyl)-4-methyl-N-phenylbenzenesulfonamide

Chemical Property:

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Technology Process of N-((1,1-dimethyl-1H-inden-2-yl)methyl)-4-methyl-N-phenylbenzenesulfonamide

There total 7 articles about N-((1,1-dimethyl-1H-inden-2-yl)methyl)-4-methyl-N-phenylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1499077-03-0
N-((1,1-dimethyl-1H-inden-2-yl)methyl)aniline

: 98-59-9
p-toluenesulfonyl chloride

: 1499076-71-9
N-((1,1-dimethyl-1H-inden-2-yl)methyl)-4-methyl-N-phenylbenzenesulfonamide

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1002/anie.201304845

Reference yield:

: 26465-81-6
3,3-dimethylindan-1-one

: 1499076-71-9
N-((1,1-dimethyl-1H-inden-2-yl)methyl)-4-methyl-N-phenylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate / methanol / 0.5 h / 20 °C

2: trichlorophosphate / 6 h / 0 - 100 °C

3: 0.25 h

4: toluene-4-sulfonic acid; benzene / 0.08 h

5: triethylamine; dmap / dichloromethane / 24 h / 20 °C

With dmap; sodium tetrahydroborate; toluene-4-sulfonic acid; triethylamine; trichlorophosphate; benzene; In methanol; dichloromethane;
DOI:10.1002/anie.201304845

Reference yield:

: 541-47-9
3-Methylbutenoic acid

: 1499076-71-9
N-((1,1-dimethyl-1H-inden-2-yl)methyl)-4-methyl-N-phenylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1: aluminum (III) chloride / 5 h / Reflux

2: sodium tetrahydroborate / methanol / 0.5 h / 20 °C

3: trichlorophosphate / 6 h / 0 - 100 °C

4: 0.25 h

5: toluene-4-sulfonic acid; benzene / 0.08 h

6: triethylamine; dmap / dichloromethane / 24 h / 20 °C

With dmap; aluminum (III) chloride; sodium tetrahydroborate; toluene-4-sulfonic acid; triethylamine; trichlorophosphate; benzene; In methanol; dichloromethane;
DOI:10.1002/anie.201304845