3-(2-Hydroxyethylthio)-4-phenylfuroxan

Base Information

Chemical Name:3-(2-Hydroxyethylthio)-4-phenylfuroxan
CAS No.:372945-80-7
Molecular Formula:C₁₀H₁₀N₂O₃S
Molecular Weight:238.267
Hs Code.:

Synonyms:3-(2-Hydroxyethylthio)-4-phenylfuroxan

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-Hydroxyethylthio)-4-phenylfuroxan

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Technology Process of 3-(2-Hydroxyethylthio)-4-phenylfuroxan

There total 1 articles about 3-(2-Hydroxyethylthio)-4-phenylfuroxan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 76016-72-3
4-phenyl-3-phenylsulfonyl furoxan

: 60-24-2
2-hydroxyethanethiol

: 372945-80-7
3-(2-Hydroxyethylthio)-4-phenylfuroxan

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; at -10 ℃; for 0.5h;
DOI:10.1039/b104845g

Reference yield: 80.0%

: 372945-80-7
3-(2-Hydroxyethylthio)-4-phenylfuroxan

: 372945-81-8
3-(2-Hydroxyethylsulfonyl)-4-phenylfuroxan

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;
DOI:10.1016/j.ejmech.2005.05.001

Reference yield:

: 372945-80-7
3-(2-Hydroxyethylthio)-4-phenylfuroxan

: 872311-56-3
3-ethenesulfonyl-4-phenyl-furazan 2-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 20 °C

2: 88 percent / mesyl chloride; triethylamine / CH₂Cl₂ / 0 °C

With methanesulfonyl chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/j.ejmech.2005.05.001