{2-[(anthracene-9-carbonyl)-amino]-acetylamino}-acetic acid 11-(3,5-di-tert-butyl-phenoxy)-undecyl ester

Base Information

Chemical Name:{2-[(anthracene-9-carbonyl)-amino]-acetylamino}-acetic acid 11-(3,5-di-tert-butyl-phenoxy)-undecyl ester
CAS No.:335596-98-0
Molecular Formula:C₄₄H₅₈N₂O₅
Molecular Weight:694.955
Hs Code.:

{2-[(anthracene-9-carbonyl)-amino]-acetylamino}-acetic acid 11-(3,5-di-<i>tert</i>-butyl-phenoxy)-undecyl ester

Synonyms:{2-[(anthracene-9-carbonyl)-amino]-acetylamino}-acetic acid 11-(3,5-di-tert-butyl-phenoxy)-undecyl ester

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Chemical Property of {2-[(anthracene-9-carbonyl)-amino]-acetylamino}-acetic acid 11-(3,5-di-tert-butyl-phenoxy)-undecyl ester

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Technology Process of {2-[(anthracene-9-carbonyl)-amino]-acetylamino}-acetic acid 11-(3,5-di-tert-butyl-phenoxy)-undecyl ester

There total 5 articles about {2-[(anthracene-9-carbonyl)-amino]-acetylamino}-acetic acid 11-(3,5-di-tert-butyl-phenoxy)-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 383424-72-4
ethyl 2-[2-(anthracene-9-carboxamido)acetamido]acetate

: 11-(3,5-di-tert-butyl-phenoxy)-undecan-1-ol

: 335596-98-0
{2-[(anthracene-9-carbonyl)-amino]-acetylamino}-acetic acid 11-(3,5-di-tert-butyl-phenoxy)-undecyl ester

Guidance literature:: With 1,3-dichlorotetrabutyldistannoxane; In toluene; Heating;
DOI:10.1021/ja015919c

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 335596-98-0
{2-[(anthracene-9-carbonyl)-amino]-acetylamino}-acetic acid 11-(3,5-di-tert-butyl-phenoxy)-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / potassium carbonate / acetonitrile / 120 h / Heating

2: 80 percent / bis(dibutylchlorotin)oxide / toluene / Heating

With 1,3-dichlorotetrabutyldistannoxane; potassium carbonate; In toluene; acetonitrile;
DOI:10.1021/ja015919c

Reference yield:

: 723-62-6
anthracen-9-carboxylic acid

: 335596-98-0
{2-[(anthracene-9-carbonyl)-amino]-acetylamino}-acetic acid 11-(3,5-di-tert-butyl-phenoxy)-undecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / oxalyl chloride; dimethylformamide / toluene / 50 °C

2: 75 percent / triethylamine / CHCl₃ / 1 h

3: 80 percent / bis(dibutylchlorotin)oxide / toluene / Heating

With oxalyl dichloride; 1,3-dichlorotetrabutyldistannoxane; triethylamine; N,N-dimethyl-formamide; In chloroform; toluene;
DOI:10.1021/ja015919c