2,4-dideoxy-3,5-O-[(4-methoxyphenyl)methylene]-2,4-dimethyl-L-arabinitol

Base Information

Chemical Name:2,4-dideoxy-3,5-O-[(4-methoxyphenyl)methylene]-2,4-dimethyl-L-arabinitol
CAS No.:517906-83-1
Molecular Formula:C₁₅H₂₂O₄
Molecular Weight:266.337
Hs Code.:

Synonyms:2,4-dideoxy-3,5-O-[(4-methoxyphenyl)methylene]-2,4-dimethyl-L-arabinitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-dideoxy-3,5-O-[(4-methoxyphenyl)methylene]-2,4-dimethyl-L-arabinitol

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Technology Process of 2,4-dideoxy-3,5-O-[(4-methoxyphenyl)methylene]-2,4-dimethyl-L-arabinitol

There total 8 articles about 2,4-dideoxy-3,5-O-[(4-methoxyphenyl)methylene]-2,4-dimethyl-L-arabinitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 947613-25-4
C₂₅H₂₉NO₆

: 517906-83-1
2,4-dideoxy-3,5-O-[(4-methoxyphenyl)methylene]-2,4-dimethyl-L-arabinitol

Guidance literature:: With lithium borohydride; In tetrahydrofuran; ethanol; at 20 ℃; for 4h;
DOI:10.1002/anie.200605198

Reference yield:

: 398518-78-0
2-[(4R,5S,6S)-2-(4-methoxyphenyl)-5-methyl-[1,3]dioxin-4-yl]propionaldehyde

: 517906-83-1
2,4-dideoxy-3,5-O-[(4-methoxyphenyl)methylene]-2,4-dimethyl-L-arabinitol

Guidance literature:: With sodium hydroxide; LiAlH₄; In tetrahydrofuran; water;

Reference yield:

: 132969-60-9
(2S)-3-[(4-methoxybenzyl)oxy]-2-methylpropanal

: 517906-83-1
2,4-dideoxy-3,5-O-[(4-methoxyphenyl)methylene]-2,4-dimethyl-L-arabinitol

Guidance literature:: Multi-step reaction with 3 steps

1.1: Bu₂BOTf; NEt₃ / CH₂Cl₂ / 0.75 h / 0 °C

1.2: 85 percent / CH₂Cl₂ / 1 h / 0 °C

2.1: 73 percent / 2,3-dichloro-5,6-dicyan-1,4-benzoquinone; 4 Angstroem molecular sieves / CH₂Cl₂ / 1.5 h / 0 °C

3.1: LiBH₄ / ethanol; tetrahydrofuran / 4 h / 20 °C

With lithium borohydride; 4 A molecular sieve; di-n-butylboryl trifluoromethanesulfonate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; ethanol; dichloromethane; 1.2: Evans aldol reaction;
DOI:10.1002/anie.200605198