1-[(1S)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]-N-(2-ethynylphenyl)-N-propadienylmethanesulfonamide

Base Information

• Chemical Name: 1-[(1S)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]-N-(2-ethynylphenyl)-N-propadienylmethanesulfonamide
• CAS No.: 1196979-10-8
• Molecular Formula: C₂₁H₂₃NO₃S
• Molecular Weight: 369.485
• Mol file: 1196979-10-8.mol

Synonyms:1-[(1S)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]-N-(2-ethynylphenyl)-N-propadienylmethanesulfonamide

Chemical Property of 1-[(1S)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]-N-(2-ethynylphenyl)-N-propadienylmethanesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1-[(1S)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]-N-(2-ethynylphenyl)-N-propadienylmethanesulfonamide

There total 1 articles about 1-[(1S)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]-N-(2-ethynylphenyl)-N-propadienylmethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-[(1S)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]-N-(2-ethynylphenyl)-N-(prop-2-yn-1-yl)methanesulfonamide (1196979-32-4) → 1-[(1S)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]-N-(2-ethynylphenyl)-N-propadienylmethanesulfonamide (1196979-10-8)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1002/ejoc.200900745

upstream raw materials:

1-[(1S)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]-N-(2-ethynylphenyl)-N-(prop-2-yn-1-yl)methanesulfonamide