Technology Process of C26H15F6N5O2
There total 6 articles about C26H15F6N5O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
tetrakis(triphenylphosphine) palladium(0);
In
N,N-dimethyl-formamide;
at 120 ℃;
for 0.333333h;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / dimethyl sulfoxide / 2 h / 40 °C
2: sodium tetrahydroborate / ethanol / 0 °C
3: iodine; sodium carbonate / methanol / 20 °C
4: thionyl chloride / chloroform / 20 - 40 °C
5: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 0.33 h / 120 °C / Microwave irradiation
With
sodium tetrahydroborate; thionyl chloride; iodine; sodium carbonate; potassium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
methanol; ethanol; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium tetrahydroborate / ethanol / 0 °C
2: iodine; sodium carbonate / methanol / 20 °C
3: thionyl chloride / chloroform / 20 - 40 °C
4: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 0.33 h / 120 °C / Microwave irradiation
With
sodium tetrahydroborate; thionyl chloride; iodine; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
methanol; ethanol; chloroform; N,N-dimethyl-formamide;