1,4-bis(chloro--methyl)-2-methoxybenzene

Base Information

Chemical Name:1,4-bis(chloro--methyl)-2-methoxybenzene
CAS No.:79237-00-6
Molecular Formula:C₉H₁₀Cl₂O
Molecular Weight:209.052
Hs Code.:

1,4-bis(chloro-<D2>-methyl)-2-methoxybenzene

Synonyms:1,4-bis(chloro--methyl)-2-methoxybenzene

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Chemical Property of 1,4-bis(chloro--methyl)-2-methoxybenzene

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Technology Process of 1,4-bis(chloro--methyl)-2-methoxybenzene

There total 2 articles about 1,4-bis(chloro--methyl)-2-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 79236-95-6
1,4-bis(hydroxy--methyl)-2-methoxybenzene

: 79237-00-6
1,4-bis(chloro--methyl)-2-methoxybenzene

Guidance literature:: With thionyl chloride; In dichloromethane; for 1h;
DOI:10.1016/S0040-4020(01)92456-1

Reference yield:

: 36727-17-0
1,4-dimethyl 2-methoxybenzene-1,4-dicarboxylate

: 79237-00-6
1,4-bis(chloro--methyl)-2-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / LiAlD₄ / tetrahydrofuran / 1 h / Heating

2: 57 percent / SOCl₂ / CH₂Cl₂ / 1 h

With thionyl chloride; lithium aluminium deuteride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)92456-1

Reference yield:

: 79237-00-6
1,4-bis(chloro--methyl)-2-methoxybenzene

: 79237-19-7
3-t-butyl-1-(7-methoxy<2,2,9,9-D4><2.2>paracyclophan-4-yl)-5--phenylformazan

Guidance literature:: Multi-step reaction with 5 steps

1: 51 percent / KOH / benzene; ethanol / 1 h / Heating

2: 82 percent / various solvent(s) / 6 h / Irradiation

3: 26 percent / conc HNO₃ / acetic acid / 1 h / Ambient temperature

4: 74 percent / H₂ / Raney Ni / ethyl acetate

5: 1.) NaNO₂; 2.) NaOAc / 1.) DMF, H₂O, conc. HCl, 0 deg C; 2.) 0 deg C, 1 h

With potassium hydroxide; hydrogen; nitric acid; sodium acetate; sodium nitrite; nickel; In ethanol; acetic acid; ethyl acetate; benzene;
DOI:10.1016/S0040-4020(01)92456-1