(S)-1-(tert-butyldiphenylsiloxy)-2-(4-methoxybenzyloxymethyl)-3-pentanone

Base Information

Chemical Name:(S)-1-(tert-butyldiphenylsiloxy)-2-(4-methoxybenzyloxymethyl)-3-pentanone
CAS No.:680201-67-6
Molecular Formula:C₃₀H₃₈O₄Si
Molecular Weight:490.715
Hs Code.:

Synonyms:(S)-1-(tert-butyldiphenylsiloxy)-2-(4-methoxybenzyloxymethyl)-3-pentanone

Suppliers and Price of (S)-1-(tert-butyldiphenylsiloxy)-2-(4-methoxybenzyloxymethyl)-3-pentanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-(tert-butyldiphenylsiloxy)-2-(4-methoxybenzyloxymethyl)-3-pentanone

Chemical Property:

Purity/Quality:

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Technology Process of (S)-1-(tert-butyldiphenylsiloxy)-2-(4-methoxybenzyloxymethyl)-3-pentanone

There total 6 articles about (S)-1-(tert-butyldiphenylsiloxy)-2-(4-methoxybenzyloxymethyl)-3-pentanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 680201-81-4
(R)-2-hydroxymethyl-1-(4-methoxybenzyloxy)-3-pentanone

: 58479-61-1
tert-butylchlorodiphenylsilane

: 680201-67-6
(S)-1-(tert-butyldiphenylsiloxy)-2-(4-methoxybenzyloxymethyl)-3-pentanone

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2005.07.029

Reference yield:

: 680201-70-1
1-benzyloxy-2-(benzyloxymethyl)-3-pentanone

: 680201-67-6
(S)-1-(tert-butyldiphenylsiloxy)-2-(4-methoxybenzyloxymethyl)-3-pentanone

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd/C

2: CSA

3: 22 percent / lipase AK; vinyl acetate

4: 95 percent / imidazole / dimethylformamide

With 1H-imidazole; vinyl acetate; lipase AK; camphor-10-sulfonic acid; hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2005.07.029

Reference yield:

: 680201-69-8
1-benzyloxy-2-(benzyloxymethyl)-3-pentanol

: 680201-67-6
(S)-1-(tert-butyldiphenylsiloxy)-2-(4-methoxybenzyloxymethyl)-3-pentanone

Guidance literature:: Multi-step reaction with 5 steps

1: 69 percent / Jones reagent

2: H₂ / Pd/C

3: CSA

4: 22 percent / lipase AK; vinyl acetate

5: 95 percent / imidazole / dimethylformamide

With 1H-imidazole; vinyl acetate; jones reagent; lipase AK; camphor-10-sulfonic acid; hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide; 1: Jones oxidation;
DOI:10.1016/j.tetlet.2005.07.029