(S)-2-amino-3-(2-(4-(4-decylbenzoyl)phenyl)acetamido)-N-hexadecylpropanamide

Base Information

Chemical Name:(S)-2-amino-3-(2-(4-(4-decylbenzoyl)phenyl)acetamido)-N-hexadecylpropanamide
CAS No.:1353054-52-0
Molecular Formula:C₄₄H₇₁N₃O₃
Molecular Weight:690.066
Hs Code.:

Synonyms:(S)-2-amino-3-(2-(4-(4-decylbenzoyl)phenyl)acetamido)-N-hexadecylpropanamide

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Chemical Property of (S)-2-amino-3-(2-(4-(4-decylbenzoyl)phenyl)acetamido)-N-hexadecylpropanamide

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Technology Process of (S)-2-amino-3-(2-(4-(4-decylbenzoyl)phenyl)acetamido)-N-hexadecylpropanamide

There total 11 articles about (S)-2-amino-3-(2-(4-(4-decylbenzoyl)phenyl)acetamido)-N-hexadecylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1353054-51-9
(S)-tert-butyl 3-(2-(4-(4-decylbenzoyl)phenyl)acetamido)-1-(hexadecylamino)-1-oxo-propan-2-ylcarbamate

: 1353054-52-0
(S)-2-amino-3-(2-(4-(4-decylbenzoyl)phenyl)acetamido)-N-hexadecylpropanamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h; Darkness;
DOI:10.1016/j.bmc.2011.10.043

Reference yield:

: 193964-80-6
(4-bromophenethoxy)triisopropylsilane

: 1353054-52-0
(S)-2-amino-3-(2-(4-(4-decylbenzoyl)phenyl)acetamido)-N-hexadecylpropanamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

1.2: 1.5 h / -78 - 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

3.1: Jones reagent / acetone / 2 h / 20 °C

4.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h

4.2: 12 h / 20 °C / Darkness

5.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h

5.2: 12 h / 20 °C / Darkness

6.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C / Darkness

With Jones reagent; n-butyllithium; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane; acetone;
DOI:10.1016/j.bmc.2011.10.043

Reference yield:

: 1353054-46-2
(4-decylphenyl)(4-(2-(triisopropylsilyloxy)ethyl)phenyl)methanol

: 1353054-52-0
(S)-2-amino-3-(2-(4-(4-decylbenzoyl)phenyl)acetamido)-N-hexadecylpropanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

2.1: Jones reagent / acetone / 2 h / 20 °C

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h

3.2: 12 h / 20 °C / Darkness

4.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h

4.2: 12 h / 20 °C / Darkness

5.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C / Darkness

With Jones reagent; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.bmc.2011.10.043