1,1-dimethylethyl -<1-(cyclohexylmethyl)-2-<(trichloroacetyl)amino>-3-butenyl>carbamate

Base Information

Chemical Name:1,1-dimethylethyl -<1-(cyclohexylmethyl)-2-<(trichloroacetyl)amino>-3-butenyl>carbamate
CAS No.:146136-21-2
Molecular Formula:C₁₈H₂₉Cl₃N₂O₃
Molecular Weight:427.799
Hs Code.:

1,1-dimethylethyl <S-(E)>-<1-(cyclohexylmethyl)-2-<(trichloroacetyl)amino>-3-butenyl>carbamate

Synonyms:1,1-dimethylethyl -<1-(cyclohexylmethyl)-2-<(trichloroacetyl)amino>-3-butenyl>carbamate

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Chemical Property of 1,1-dimethylethyl -<1-(cyclohexylmethyl)-2-<(trichloroacetyl)amino>-3-butenyl>carbamate

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Technology Process of 1,1-dimethylethyl -<1-(cyclohexylmethyl)-2-<(trichloroacetyl)amino>-3-butenyl>carbamate

There total 1 articles about 1,1-dimethylethyl -<1-(cyclohexylmethyl)-2-<(trichloroacetyl)amino>-3-butenyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 146136-19-8
1,1-dimethylethyl -<1-(cyclohexylmethyl)-4-(2,2,2-trichloro-1-iminoethoxy)-2-butenyl>carbamate

: 146136-21-2
1,1-dimethylethyl -<1-(cyclohexylmethyl)-2-<(trichloroacetyl)amino>-3-butenyl>carbamate

Guidance literature:: palladium diacetate; In tetrahydrofuran; for 4h; Mechanism; Ambient temperature; other solvent; other catalysts; stereoselectivity;
DOI:10.1021/jo00055a047

Reference yield: 78.0%

: 146136-21-2
1,1-dimethylethyl -<1-(cyclohexylmethyl)-2-<(trichloroacetyl)amino>-3-butenyl>carbamate

: 146136-22-3
1,1-dimethylethyl (S)-<2-amino-1-(cyclohexylmethyl)-3-butenyl>carbamate

Guidance literature:: With sodium hydroxide; In ethanol; for 24h; Ambient temperature;
DOI:10.1021/jo00055a047

Reference yield:

: 146136-21-2
1,1-dimethylethyl -<1-(cyclohexylmethyl)-2-<(trichloroacetyl)amino>-3-butenyl>carbamate

: 1026005-82-2
(2S,3S)-1-Cyclohexyl-pent-4-ene-2,3-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 6 N aq.NaOH / aq. ethanol / 24 h / Ambient temperature

2: HCl(g) / CH₂Cl₂; methanol / 1 h

With hydrogenchloride; sodium hydroxide; In methanol; ethanol; dichloromethane;
DOI:10.1021/jo00055a047