methyl 2-acetamido-6-(benzyloxycarbonylamino)-7-chloro-2,3,4,6,7-pentadeoxy-β-L-lyxo-heptopyranoside

Base Information

Chemical Name:methyl 2-acetamido-6-(benzyloxycarbonylamino)-7-chloro-2,3,4,6,7-pentadeoxy-β-L-lyxo-heptopyranoside
CAS No.:79970-12-0
Molecular Formula:C₁₈H₂₅ClN₂O₅
Molecular Weight:384.86
Hs Code.:

Synonyms:methyl 2-acetamido-6-(benzyloxycarbonylamino)-7-chloro-2,3,4,6,7-pentadeoxy-β-L-lyxo-heptopyranoside

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Chemical Property of methyl 2-acetamido-6-(benzyloxycarbonylamino)-7-chloro-2,3,4,6,7-pentadeoxy-β-L-lyxo-heptopyranoside

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Technology Process of methyl 2-acetamido-6-(benzyloxycarbonylamino)-7-chloro-2,3,4,6,7-pentadeoxy-β-L-lyxo-heptopyranoside

There total 3 articles about methyl 2-acetamido-6-(benzyloxycarbonylamino)-7-chloro-2,3,4,6,7-pentadeoxy-β-L-lyxo-heptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68912-24-3
[2-((2S,5R,6S)-5-Acetylamino-6-methoxy-tetrahydro-pyran-2-yl)-2-hydroxy-ethyl]-carbamic acid benzyl ester

: 79970-12-0
methyl 2-acetamido-6-(benzyloxycarbonylamino)-7-chloro-2,3,4,6,7-pentadeoxy-β-L-lyxo-heptopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent

2: sodium isopropoxide / dioxane / 2 h / Heating

3: dioxane; toluene / 3 h / Heating

With sodium isopropylate; In 1,4-dioxane; toluene;
DOI:10.1246/bcsj.54.2825

Reference yield:

: 69070-77-5,79952-88-8
Methanesulfonic acid 1-((2S,5R,6S)-5-acetylamino-6-methoxy-tetrahydro-pyran-2-yl)-2-benzyloxycarbonylamino-ethyl ester

: 79970-12-0
methyl 2-acetamido-6-(benzyloxycarbonylamino)-7-chloro-2,3,4,6,7-pentadeoxy-β-L-lyxo-heptopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium isopropoxide / dioxane / 2 h / Heating

2: dioxane; toluene / 3 h / Heating

With sodium isopropylate; In 1,4-dioxane; toluene;
DOI:10.1246/bcsj.54.2825