Dibenzyl-[(1S,2R)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-2-(2-methoxy-ethoxymethoxy)-butyl]-amine

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Chemical Name:Dibenzyl-[(1S,2R)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-2-(2-methoxy-ethoxymethoxy)-butyl]-amine
CAS No.:613264-64-5
Molecular Formula:C₃₁H₅₁NO₄Si
Molecular Weight:529.836
Hs Code.:

Synonyms:Dibenzyl-[(1S,2R)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-2-(2-methoxy-ethoxymethoxy)-butyl]-amine

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Chemical Property of Dibenzyl-[(1S,2R)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-2-(2-methoxy-ethoxymethoxy)-butyl]-amine

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Technology Process of Dibenzyl-[(1S,2R)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-2-(2-methoxy-ethoxymethoxy)-butyl]-amine

There total 2 articles about Dibenzyl-[(1S,2R)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-2-(2-methoxy-ethoxymethoxy)-butyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 613264-56-5
(3R,4S)-7-(tert-Butyl-dimethyl-silanyloxy)-4-dibenzylamino-heptan-3-ol

: 613264-64-5
Dibenzyl-[(1S,2R)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-2-(2-methoxy-ethoxymethoxy)-butyl]-amine

Guidance literature:: 2-Methoxyethoxymethyl chloride; (3R,4S)-7-(tert-Butyl-dimethyl-silanyloxy)-4-dibenzylamino-heptan-3-ol; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃;

In dichloromethane; at 20 ℃; for 16h; Further stages.;
DOI:10.1002/ejoc.200300199

Reference yield:

: 205068-02-6
(-)-S-5-(tert-butyldimethylsilyloxy)-2-(N,N-dibenzylamino)-1-pentanal

: 613264-64-5
Dibenzyl-[(1S,2R)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-2-(2-methoxy-ethoxymethoxy)-butyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 73 percent / diethyl ether / 1 h / 0 °C

2.1: diisopropylethylamine / CH₂Cl₂ / 0 °C

2.2: 70 percent / CH₂Cl₂ / 16 h / 20 °C

With N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane;
DOI:10.1002/ejoc.200300199