C₃₉H₄₂N₈O₈S

Base Information

Chemical Name:C₃₉H₄₂N₈O₈S
CAS No.:952413-92-2
Molecular Formula:C₃₉H₄₂N₈O₈S
Molecular Weight:782.877
Hs Code.:

C<sub>39</sub>H<sub>42</sub>N<sub>8</sub>O<sub>8</sub>S

Synonyms:C₃₉H₄₂N₈O₈S

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Chemical Property of C₃₉H₄₂N₈O₈S

Chemical Property:

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Technology Process of C₃₉H₄₂N₈O₈S

There total 6 articles about C₃₉H₄₂N₈O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930285-04-4
methyl 2'-(2-bromo-1,1-dimethoxyethyl)-5-phenyl-[2,4']bis-oxazolyl-4-carboxylate

: 952413-92-2
C₃₉H₄₂N₈O₈S

Guidance literature:: Multi-step reaction with 7 steps

1.1: 91 percent / formic acid / 2 h / Heating

2.1: NaHCO₃ / tetrahydrofuran / 8 h / 20 °C

2.2: 62 percent / TFAA; lutidine / tetrahydrofuran / -10 - 20 °C

3.1: 100 percent / LiOH / tetrahydrofuran; H₂O; methanol / 1 h / 20 °C

4.1: 70 percent / EDC*HCl; HOBt; N,N-diisopropylethylamine / CH₂Cl₂ / 0 - 20 °C

5.1: LiOH / tetrahydrofuran; H₂O; methanol / 1 h / 20 °C

6.1: EDC*HCl; N,N-diisopropylethylamine / tetrahydrofuran; dimethylformamide / 0 - 20 °C

7.1: trifluoroacetic acid / CH₂Cl₂ / 1 h / 20 °C

7.2: 10 mg / N,N-diisopropylethylamine / tetrahydrofuran / 96 h / 20 °C

With lithium hydroxide; formic acid; sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 2.2: Hantzsch thiazole synthesis;
DOI:10.1016/j.tet.2007.06.103

Reference yield:

: C₄₄H₅₂N₈O₁₁S

: 952413-92-2
C₃₉H₄₂N₈O₈S

Guidance literature:: Multi-step reaction with 2 steps

1.1: EDC*HCl; N,N-diisopropylethylamine / tetrahydrofuran; dimethylformamide / 0 - 20 °C

2.1: trifluoroacetic acid / CH₂Cl₂ / 1 h / 20 °C

2.2: 10 mg / N,N-diisopropylethylamine / tetrahydrofuran / 96 h / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.06.103

Reference yield:

: 952413-85-3
C₃₃H₃₂N₆O₉S

: 952413-92-2
C₃₉H₄₂N₈O₈S

Guidance literature:: Multi-step reaction with 4 steps

1.1: 70 percent / EDC*HCl; HOBt; N,N-diisopropylethylamine / CH₂Cl₂ / 0 - 20 °C

2.1: LiOH / tetrahydrofuran; H₂O; methanol / 1 h / 20 °C

3.1: EDC*HCl; N,N-diisopropylethylamine / tetrahydrofuran; dimethylformamide / 0 - 20 °C

4.1: trifluoroacetic acid / CH₂Cl₂ / 1 h / 20 °C

4.2: 10 mg / N,N-diisopropylethylamine / tetrahydrofuran / 96 h / 20 °C

With lithium hydroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.06.103