3-azido-4-methylbenzyl iodide

Base Information

Chemical Name:3-azido-4-methylbenzyl iodide
CAS No.:902140-56-1
Molecular Formula:C₈H₈IN₃
Molecular Weight:273.076
Hs Code.:

Synonyms:3-azido-4-methylbenzyl iodide

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Chemical Property of 3-azido-4-methylbenzyl iodide

Chemical Property:

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Technology Process of 3-azido-4-methylbenzyl iodide

There total 3 articles about 3-azido-4-methylbenzyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 902140-55-0
3-azido-4-methylbenzyl chloride

: 902140-56-1
3-azido-4-methylbenzyl iodide

Guidance literature:: With sodium iodide; In acetone; at 20 ℃; for 12h;
DOI:10.1016/j.tet.2006.04.056

Reference yield:

: 902140-54-9
3-azido-4-methylbenzyl alcohol

: 902140-56-1
3-azido-4-methylbenzyl iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / thionyl chloride / CH₂Cl₂ / 3 h / 0 °C

2: 87 percent / sodium iodide / acetone / 12 h / 20 °C

With thionyl chloride; sodium iodide; In dichloromethane; acetone;
DOI:10.1016/j.tet.2006.04.056

Reference yield:

: 81863-45-8
3-(hydroxymethyl)-6-methylaniline

: 902140-56-1
3-azido-4-methylbenzyl iodide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium nitrite; sulfuric acid / H₂O / 0.5 h / cooling

1.2: 82 percent / sodium azide / H₂O / 16 h / 20 °C

2.1: 84 percent / thionyl chloride / CH₂Cl₂ / 3 h / 0 °C

3.1: 87 percent / sodium iodide / acetone / 12 h / 20 °C

With thionyl chloride; sulfuric acid; sodium iodide; sodium nitrite; In dichloromethane; water; acetone;
DOI:10.1016/j.tet.2006.04.056