N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-benzylhydrazine

Base Information

Chemical Name:N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-benzylhydrazine
CAS No.:886055-98-7
Molecular Formula:C₂₆H₃₃FN₂O₄
Molecular Weight:456.557
Hs Code.:

Synonyms:N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-benzylhydrazine

Suppliers and Price of N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-benzylhydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-benzylhydrazine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-benzylhydrazine

There total 3 articles about N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-benzylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 843651-78-5
N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]hydrazine

: 886055-98-7
N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-benzylhydrazine

Guidance literature:: N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]hydrazine; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

benzyl halide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jm050538l

Reference yield:

: 350-40-3
2-(4-fluorophenyl)-1-propene

: 886055-98-7
N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-benzylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: NBS / CCl₄ / Heating

2.1: NaH / dimethylformamide / 0.33 h / 20 °C

2.2: 89 percent / dimethylformamide / 7 h / 20 °C

3.1: NaH / dimethylformamide / 0.33 h / 20 °C

3.2: 70 percent / dimethylformamide / 20 °C

With N-Bromosuccinimide; sodium hydride; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050538l

Reference yield:

: 132927-05-0
1-(3-bromoprop-1-en-2-yl)-4-fluorobenzene

: 886055-98-7
N,N'-di(tert-butoxycarbonyl)-N'-[2-(4-fluorophenyl)allyl]-N-benzylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.33 h / 20 °C

1.2: 89 percent / dimethylformamide / 7 h / 20 °C

2.1: NaH / dimethylformamide / 0.33 h / 20 °C

2.2: 70 percent / dimethylformamide / 20 °C

With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jm050538l