5-<1-Hydroxy-1-(3',4',5'-trimethoxyphenyl)methyl>-6-trimethylsilylmethyl-1,3-benzodioxole

Base Information

Chemical Name:5-<1-Hydroxy-1-(3',4',5'-trimethoxyphenyl)methyl>-6-trimethylsilylmethyl-1,3-benzodioxole
CAS No.:98151-84-9
Molecular Formula:C₂₁H₂₈O₆Si
Molecular Weight:404.535
Hs Code.:

Synonyms:5-<1-Hydroxy-1-(3',4',5'-trimethoxyphenyl)methyl>-6-trimethylsilylmethyl-1,3-benzodioxole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-<1-Hydroxy-1-(3',4',5'-trimethoxyphenyl)methyl>-6-trimethylsilylmethyl-1,3-benzodioxole

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Technology Process of 5-<1-Hydroxy-1-(3',4',5'-trimethoxyphenyl)methyl>-6-trimethylsilylmethyl-1,3-benzodioxole

There total 5 articles about 5-<1-Hydroxy-1-(3',4',5'-trimethoxyphenyl)methyl>-6-trimethylsilylmethyl-1,3-benzodioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 98151-83-8
5-Bromo-6-trimethylsilylmethyl-1,3-benzodioxole

: 98151-84-9
5-<1-Hydroxy-1-(3',4',5'-trimethoxyphenyl)methyl>-6-trimethylsilylmethyl-1,3-benzodioxole

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 ℃;
DOI:10.1039/c39850000485

Reference yield:

: 98151-82-7
<(3,4-methylenedioxyphenyl)methyl>trimethylsilane

: 98151-84-9
5-<1-Hydroxy-1-(3',4',5'-trimethoxyphenyl)methyl>-6-trimethylsilylmethyl-1,3-benzodioxole

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Br₂, 5percent aq. NaHCO₃ / CH₂Cl₂

2: 92 percent / 1.) n-BuLi / tetrahydrofuran / -78 °C

With n-butyllithium; bromine; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c39850000485