(1-benzyl-2-oxocyclohexyl)methyl diethoxyphosphinylacetate

Base Information

Chemical Name:(1-benzyl-2-oxocyclohexyl)methyl diethoxyphosphinylacetate
CAS No.:936836-55-4
Molecular Formula:C₂₀H₂₉O₆P
Molecular Weight:396.42
Hs Code.:

Synonyms:(1-benzyl-2-oxocyclohexyl)methyl diethoxyphosphinylacetate

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Chemical Property of (1-benzyl-2-oxocyclohexyl)methyl diethoxyphosphinylacetate

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Technology Process of (1-benzyl-2-oxocyclohexyl)methyl diethoxyphosphinylacetate

There total 4 articles about (1-benzyl-2-oxocyclohexyl)methyl diethoxyphosphinylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 862202-17-3
2-benzyl-2-hydroxymethylcyclohexanone

: 3095-95-2
diethylphosphonoacetic acid

: 936836-55-4
(1-benzyl-2-oxocyclohexyl)methyl diethoxyphosphinylacetate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2007.02.027

Reference yield:

: (6-benzyl-1,4-dioxa-spiro[4.5]dec-6-yl)-methanol

: 936836-55-4
(1-benzyl-2-oxocyclohexyl)methyl diethoxyphosphinylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 3.49 g / HCl; H₂O / diethyl ether / 2 h / 20 °C

2: 86 percent / DMAP; dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / 20 °C

With hydrogenchloride; dmap; water; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2007.02.027

Reference yield:

: 936836-51-0
ethyl 1-benzyl-(2,2-ethylenedioxy)cyclohexanecarboxylate

: 936836-55-4
(1-benzyl-2-oxocyclohexyl)methyl diethoxyphosphinylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether / 0 °C

2: 3.49 g / HCl; H₂O / diethyl ether / 2 h / 20 °C

3: 86 percent / DMAP; dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / 20 °C

With hydrogenchloride; dmap; lithium aluminium tetrahydride; water; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2007.02.027