methyl 2,3,4-tri-O-benzyl-(6R)-C-methyl-6-O-(2,3,4-tri-O-benzyl-α-D-glycopyranosyl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzyl-(6R)-C-methyl-6-O-(2,3,4-tri-O-benzyl-α-D-glycopyranosyl)-α-D-glucopyranoside
CAS No.:341496-15-9
Molecular Formula:C₅₆H₆₂O₁₁
Molecular Weight:911.102
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzyl-(6R)-C-methyl-6-O-(2,3,4-tri-O-benzyl-α-D-glycopyranosyl)-α-D-glucopyranoside

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Chemical Property of methyl 2,3,4-tri-O-benzyl-(6R)-C-methyl-6-O-(2,3,4-tri-O-benzyl-α-D-glycopyranosyl)-α-D-glucopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzyl-(6R)-C-methyl-6-O-(2,3,4-tri-O-benzyl-α-D-glycopyranosyl)-α-D-glucopyranoside

There total 10 articles about methyl 2,3,4-tri-O-benzyl-(6R)-C-methyl-6-O-(2,3,4-tri-O-benzyl-α-D-glycopyranosyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 341495-99-6
methyl 6-O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzyl-(6R)-C-methyl-α-D-glucopyranoside

: 341496-15-9
methyl 2,3,4-tri-O-benzyl-(6R)-C-methyl-6-O-(2,3,4-tri-O-benzyl-α-D-glycopyranosyl)-α-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1139/v01-005

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 341496-15-9
methyl 2,3,4-tri-O-benzyl-(6R)-C-methyl-6-O-(2,3,4-tri-O-benzyl-α-D-glycopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1.1: 70 percent / CrO₃; pyridine / CH₂Cl₂ / 0.17 h / 20 °C

2.1: diethyl ether / 2 h / 20 °C

2.2: pyridine; 4-dimethylaminopyridine / 20 °C

3.1: NaOH / dioxane; H₂O

4.1: 59 percent / tetraethylammonium bromide; N,N-dimethylformamide / CH₂Cl₂

5.1: 83 percent / NaOMe / methanol

With pyridine; chromium(VI) oxide; sodium hydroxide; tetraethylammonium bromide; sodium methylate; N,N-dimethyl-formamide; In 1,4-dioxane; methanol; diethyl ether; dichloromethane; water; 2.1: Grignard reaction;
DOI:10.1139/v01-005

Reference yield:

: 83051-88-1
methyl 6-aldehydo-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 341496-15-9
methyl 2,3,4-tri-O-benzyl-(6R)-C-methyl-6-O-(2,3,4-tri-O-benzyl-α-D-glycopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: diethyl ether / 2 h / 20 °C

1.2: pyridine; 4-dimethylaminopyridine / 20 °C

2.1: NaOH / dioxane; H₂O

3.1: 59 percent / tetraethylammonium bromide; N,N-dimethylformamide / CH₂Cl₂

4.1: 83 percent / NaOMe / methanol

With sodium hydroxide; tetraethylammonium bromide; sodium methylate; N,N-dimethyl-formamide; In 1,4-dioxane; methanol; diethyl ether; dichloromethane; water; 1.1: Grignard reaction;
DOI:10.1139/v01-005