5-azidopentyl 4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalamido-β-D-glucopyranoside

Base Information

Chemical Name:5-azidopentyl 4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalamido-β-D-glucopyranoside
CAS No.:1169693-77-9
Molecular Formula:C₃₅H₃₈N₄O₈
Molecular Weight:642.709
Hs Code.:

Synonyms:5-azidopentyl 4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalamido-β-D-glucopyranoside

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Chemical Property of 5-azidopentyl 4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalamido-β-D-glucopyranoside

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Technology Process of 5-azidopentyl 4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalamido-β-D-glucopyranoside

There total 2 articles about 5-azidopentyl 4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalamido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1219717-78-8
C₃₇H₃₅NO₇S

: 170220-11-8
5-azido-1-pentanol

: 1169693-77-9
5-azidopentyl 4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalamido-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In diethyl ether; dichloromethane; at -40 - 20 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.200903035

Reference yield: 90.0%

: 1169693-74-6
4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalamido-β-D-glucopyranoside N-phenyl trifluoroacetimidate

: 170220-11-8
5-azido-1-pentanol

: 1169693-77-9
5-azidopentyl 4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalamido-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; Molecular sieve;
DOI:10.1016/j.tetasy.2009.02.028

Reference yield: 95.0%

: 1169693-77-9
5-azidopentyl 4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalamido-β-D-glucopyranoside

: 1169693-80-4
5-azidopentyl-O-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: 5-azidopentyl 4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalamido-β-D-glucopyranoside; With sodium methylate; In methanol; at 20 ℃; for 2h;

With Amberlite IR-120; In methanol;
DOI:10.1016/j.tetasy.2009.02.028