C₃₆H₃₇NO₅

Base Information

Chemical Name:C₃₆H₃₇NO₅
CAS No.:1379450-00-6
Molecular Formula:C₃₆H₃₇NO₅
Molecular Weight:563.693
Hs Code.:

C<sub>36</sub>H<sub>37</sub>NO<sub>5</sub>

Synonyms:C₃₆H₃₇NO₅

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Chemical Property of C₃₆H₃₇NO₅

Chemical Property:

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Technology Process of C₃₆H₃₇NO₅

There total 9 articles about C₃₆H₃₇NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1379449-99-6
C₄₂H₅₁NO₅Si

: 1379450-00-6
C₃₆H₃₇NO₅

Guidance literature:: With ammonium fluoride; In methanol; at 25 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja301326k

Reference yield:

: 1379449-94-1
C₂₁H₃₂N₂O₆

: 1379450-00-6
C₃₆H₃₇NO₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 25 °C

3.1: tetrahydrofuran / 0 - 25 °C / Inert atmosphere; Molecular sieve

4.1: pyridinium chlorochromate / dichloromethane / 4 h / 25 °C / Inert atmosphere; Molecular sieve

5.1: 2,6-di-tert-butyl-pyridine / nitromethane / 2 h / -20 °C / Inert atmosphere; Molecular sieve

6.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride / N,N-dimethyl-formamide / 16 h / 45 °C / Inert atmosphere

7.1: trifluoroacetic acid / dichloromethane / 0 - 25 °C / Inert atmosphere

8.1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 2 h / 25 °C / Inert atmosphere

8.2: 16 h / 20 °C / Inert atmosphere

9.1: lithium aluminium tetrahydride; aluminum (III) chloride / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

10.1: ammonium fluoride / methanol / 1 h / 25 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; aluminum (III) chloride; ammonium fluoride; copper(l) iodide; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-pyridine; cesium fluoride; 1,1'-carbonyldiimidazole; pyridinium chlorochromate; trifluoroacetic acid; In tetrahydrofuran; methanol; nitromethane; dichloromethane; N,N-dimethyl-formamide; 5.1: Friedel Crafts acylation / 6.1: Stille coupling;
DOI:10.1021/ja301326k

Reference yield:

: 1379449-81-6
C₁₈H₂₈N₂O₆

: 1379450-00-6
C₃₆H₃₇NO₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 6 h / 0 °C

2.1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 25 °C

4.1: tetrahydrofuran / 0 - 25 °C / Inert atmosphere; Molecular sieve

5.1: pyridinium chlorochromate / dichloromethane / 4 h / 25 °C / Inert atmosphere; Molecular sieve

6.1: 2,6-di-tert-butyl-pyridine / nitromethane / 2 h / -20 °C / Inert atmosphere; Molecular sieve

7.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride / N,N-dimethyl-formamide / 16 h / 45 °C / Inert atmosphere

8.1: trifluoroacetic acid / dichloromethane / 0 - 25 °C / Inert atmosphere

9.1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 2 h / 25 °C / Inert atmosphere

9.2: 16 h / 20 °C / Inert atmosphere

10.1: lithium aluminium tetrahydride; aluminum (III) chloride / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

11.1: ammonium fluoride / methanol / 1 h / 25 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; aluminum (III) chloride; ammonium fluoride; copper(l) iodide; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-pyridine; sodium hydride; cesium fluoride; 1,1'-carbonyldiimidazole; pyridinium chlorochromate; trifluoroacetic acid; In tetrahydrofuran; methanol; nitromethane; dichloromethane; N,N-dimethyl-formamide; 6.1: Friedel Crafts acylation / 7.1: Stille coupling;
DOI:10.1021/ja301326k