1-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

Base Information

Chemical Name:1-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane
CAS No.:1580435-99-9
Molecular Formula:C₁₈H₂₈B₁₀O₅
Molecular Weight:432.527
Hs Code.:

Synonyms:1-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

Suppliers and Price of 1-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

There total 2 articles about 1-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 17702-41-9
nido-decaborane

: 185698-55-9
2-(3-hydroxy-4-methoxyphenyl)-1-(3',4',5'-trimethoxyphenyl)ethyne

: 1580435-99-9
1-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

Guidance literature:: With N,N-dimethyl-aniline; In chlorobenzene; at 120 ℃; for 0.25h; Reagent/catalyst; Solvent; Temperature; Time; Microwave irradiation; Inert atmosphere;
DOI:10.1039/c3dt52828f

Reference yield:

: 53560-33-1
3,4,5-trimethoxyphenylacetylene

: 160257-85-2
5-iodo-2-methoxyphenol

: 1580435-99-9
1-(3-hydroxy-4-methoxyphenyl)-2-(3,4,5-trimethoxyphenyl)-ortho-carborane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 4 - 6 h / Reflux

2: N,N-dimethyl-aniline / chlorobenzene / 0.25 h / 120 °C / Microwave irradiation; Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-aniline; In tetrahydrofuran; chlorobenzene; 1: |Sonogashira Cross-Coupling;
DOI:10.1039/c3dt52828f