10-(benzoyloxy)-2-hydroxydecanoic acid

Base Information

Chemical Name:10-(benzoyloxy)-2-hydroxydecanoic acid
CAS No.:1400695-51-3
Molecular Formula:C₁₇H₂₄O₅
Molecular Weight:308.375
Hs Code.:

Synonyms:10-(benzoyloxy)-2-hydroxydecanoic acid

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Chemical Property of 10-(benzoyloxy)-2-hydroxydecanoic acid

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Technology Process of 10-(benzoyloxy)-2-hydroxydecanoic acid

There total 2 articles about 10-(benzoyloxy)-2-hydroxydecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1400695-35-3
10-(benzoyloxy)-decane-1,2-diol

: 1400695-51-3
10-(benzoyloxy)-2-hydroxydecanoic acid

Guidance literature:: 10-(benzoyloxy)-decane-1,2-diol; With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In aq. phosphate buffer; toluene; at 25 ℃; pH=6.8;

With sodium hypochlorite; sodium chlorite; In aq. phosphate buffer; toluene; at 50 ℃; for 1.5h; chemoselective reaction;
DOI:10.1021/acs.orglett.5b01003

Reference yield:

: 94108-33-5
dec-9-en-1-yl benzoate

: 1400695-51-3
10-(benzoyloxy)-2-hydroxydecanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: bis(pinacol)diborane; caesium carbonate; methanol / tetrahydrofuran / 6 h / 70 °C

1.2: 1 h / 0 °C

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / toluene; aq. phosphate buffer / 25 °C / pH 6.8

2.2: 1.5 h / 50 °C

With methanol; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; caesium carbonate; bis(pinacol)diborane; In tetrahydrofuran; aq. phosphate buffer; toluene;
DOI:10.1021/acs.orglett.5b01003

Reference yield: 77.0%

: 1400695-51-3
10-(benzoyloxy)-2-hydroxydecanoic acid

: 1400695-52-4
10-(benzoyloxy)-2-oxodecanoic acid

Guidance literature:: With 2-azatricyclo[3.3.1.1^3,7]dec-2-yloxidanyl; sodium nitrite; In aq. phosphate buffer; water; acetonitrile; at 25 ℃; for 2h; chemoselective reaction;
DOI:10.1021/acs.orglett.6b01964