PhB(2,6-(i)Pr₂C₆H₃N)2(Cl)SiSi(H)(2,6-(i)Pr₂C₆H₃N)2BPh

Base Information

• Chemical Name: PhB(2,6-(i)Pr₂C₆H₃N)2(Cl)SiSi(H)(2,6-(i)Pr₂C₆H₃N)2BPh
• CAS No.: 1186032-01-8
• Molecular Formula: C₆₀H₇₉B₂ClN₄Si₂
• Molecular Weight: 969.56
• Mol file: 1186032-01-8.mol

Synonyms:PhB(2,6-(i)Pr₂C₆H₃N)2(Cl)SiSi(H)(2,6-(i)Pr₂C₆H₃N)2BPh

Chemical Property of PhB(2,6-(i)Pr₂C₆H₃N)2(Cl)SiSi(H)(2,6-(i)Pr₂C₆H₃N)2BPh

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of PhB(2,6-(i)Pr₂C₆H₃N)2(Cl)SiSi(H)(2,6-(i)Pr₂C₆H₃N)2BPh

There total 1 articles about PhB(2,6-(i)Pr₂C₆H₃N)2(Cl)SiSi(H)(2,6-(i)Pr₂C₆H₃N)2BPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.5%

[PhB(2,6-(i)Pr2C6H3N)2]SiHCl (1186031-98-0) → PhB(2,6-(i)Pr2C6H3N)2(Cl)SiSi(H)(2,6-(i)Pr2C6H3N)2BPh (1186032-01-8)

Guidance literature:

With 1,3-bis(tert-butyl)imidazol-2-ylidene; In hexane; under Ar or N2; a soln. of I(t-Bu) (2.0 mmol) in n-hexane was added to asoln. of B-contg. compd. (4.0 mmol) in n-hexane; stirring at room temp. for 12 h; the ppt. was filtered and filtrate was concd. and stored at -40°Cfor 24 h; elem. anal.;

DOI:10.1021/om900444z

upstream raw materials:

[PhB(2,6-(i)Pr₂C₆H₃N)2]SiHCl