3,3'-dibenzoylisophthalophenone tetrahydrazone

Base Information

Chemical Name:3,3'-dibenzoylisophthalophenone tetrahydrazone
CAS No.:85566-10-5
Molecular Formula:C₃₄H₃₀N₈
Molecular Weight:550.666
Hs Code.:

Synonyms:3,3'-dibenzoylisophthalophenone tetrahydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3'-dibenzoylisophthalophenone tetrahydrazone

Chemical Property:

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Technology Process of 3,3'-dibenzoylisophthalophenone tetrahydrazone

There total 8 articles about 3,3'-dibenzoylisophthalophenone tetrahydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 85566-09-2
[3-(3-Benzoyl-benzoyl)-phenyl]-(3-benzoyl-phenyl)-methanone

: 85566-10-5
3,3'-dibenzoylisophthalophenone tetrahydrazone

Guidance literature:: With hydrazine hydrate; In ethanol;
DOI:10.1021/ja00349a068

Reference yield:

: 626-17-5
benzene-1,3-dicarbonitrile

: 85566-10-5
3,3'-dibenzoylisophthalophenone tetrahydrazone

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / Mg / diethyl ether; benzene / 1.) 0 deg C up to RT; 2.) RT, 1 h

2: 100 percent / sodium dichromate / acetic acid / 70 h / Heating

3: 80 percent / aq. KOH, KMnO₄ / 1.5 h / Heating

4: 100 percent / thionyl chloride / 8 h / Heating

5: 78 percent / AlCl₃ / 1.) 0 deg C up to RT; 2.) RT, 3 h

6: 79 percent / hydrazine hydrate / ethanol / 40 h / Heating

With potassium hydroxide; potassium permanganate; aluminium trichloride; thionyl chloride; sodium dichromate; hydrazine hydrate; magnesium; In diethyl ether; ethanol; acetic acid; benzene;
DOI:10.1021/ja00269a005

Reference yield:

: 85566-07-0
isophthalophenone-3,3'-dicarboxylic acid

: 85566-10-5
3,3'-dibenzoylisophthalophenone tetrahydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / thionyl chloride / 8 h / Heating

2: 78 percent / AlCl₃ / 1.) 0 deg C up to RT; 2.) RT, 3 h

3: 79 percent / hydrazine hydrate / ethanol / 40 h / Heating

With aluminium trichloride; thionyl chloride; hydrazine hydrate; In ethanol;
DOI:10.1021/ja00269a005