8,10-diphenyl-7,11-dipropyl-7,11-dihydrobenzo[a]benzo[5,6]quinolino[2,3,4-kl]acridin-17c-ylium tetrafluoroborate

Base Information

Chemical Name:8,10-diphenyl-7,11-dipropyl-7,11-dihydrobenzo[a]benzo[5,6]quinolino[2,3,4-kl]acridin-17c-ylium tetrafluoroborate
CAS No.:1452922-36-9
Molecular Formula:BF₄*C₄₅H₃₇N₂
Molecular Weight:692.607
Hs Code.:

Synonyms:8,10-diphenyl-7,11-dipropyl-7,11-dihydrobenzo[a]benzo[5,6]quinolino[2,3,4-kl]acridin-17c-ylium tetrafluoroborate

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Chemical Property of 8,10-diphenyl-7,11-dipropyl-7,11-dihydrobenzo[a]benzo[5,6]quinolino[2,3,4-kl]acridin-17c-ylium tetrafluoroborate

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Technology Process of 8,10-diphenyl-7,11-dipropyl-7,11-dihydrobenzo[a]benzo[5,6]quinolino[2,3,4-kl]acridin-17c-ylium tetrafluoroborate

There total 10 articles about 8,10-diphenyl-7,11-dipropyl-7,11-dihydrobenzo[a]benzo[5,6]quinolino[2,3,4-kl]acridin-17c-ylium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1452922-30-3
8,10-dibromo-7,11-dipropyl-7,11-dihydrobenzo[a]benzo[5,6]quinolino[2,3,4-kl]acridin-17c-ylium tetrafluoroborate

: 98-80-6
phenylboronic acid

: 1452922-36-9
8,10-diphenyl-7,11-dipropyl-7,11-dihydrobenzo[a]benzo[5,6]quinolino[2,3,4-kl]acridin-17c-ylium tetrafluoroborate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; at 80 ℃; for 15h; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201208926

Reference yield:

: 1452922-08-5
11-methoxy-12H-benzo[a]xanthen-12-one

: 1452922-36-9
8,10-diphenyl-7,11-dipropyl-7,11-dihydrobenzo[a]benzo[5,6]quinolino[2,3,4-kl]acridin-17c-ylium tetrafluoroborate

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / diethyl ether; hexane / 2 h / -78 - 25 °C / Inert atmosphere

1.2: -78 - 25 °C / Inert atmosphere

1.3: 0.08 h

2.1: 1-methyl-pyrrolidin-2-one / 0.17 h / 170 °C / Microwave irradiation; Inert atmosphere

3.1: acetic acid; N-Bromosuccinimide / chloroform / 15 h / 25 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,4-dioxane / 15 h / 80 °C / Schlenk technique; Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; acetic acid; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; diethyl ether; hexane; chloroform; 4.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/anie.201208926

Reference yield:

: 1452922-10-9
11-methoxy-12-(2-methoxynaphthalen-1-yl)-12H-benzo[a]xanthen-12-ylium tetrafluoroborate

: 1452922-36-9
8,10-diphenyl-7,11-dipropyl-7,11-dihydrobenzo[a]benzo[5,6]quinolino[2,3,4-kl]acridin-17c-ylium tetrafluoroborate

Guidance literature:: Multi-step reaction with 3 steps

1: 1-methyl-pyrrolidin-2-one / 0.17 h / 170 °C / Microwave irradiation; Inert atmosphere

2: acetic acid; N-Bromosuccinimide / chloroform / 15 h / 25 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,4-dioxane / 15 h / 80 °C / Schlenk technique; Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; acetic acid; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; chloroform; 3: |Suzuki-Miyaura Coupling;
DOI:10.1002/anie.201208926