(R)-allyl 4-(9,9-dimethyl-5-(naphthalen-2-ylmethyl)-(4,7-dioxo-2,8-dioxa-3,6-diazadecyl))benzylcarbamate

Base Information

Chemical Name:(R)-allyl 4-(9,9-dimethyl-5-(naphthalen-2-ylmethyl)-(4,7-dioxo-2,8-dioxa-3,6-diazadecyl))benzylcarbamate
CAS No.:1173159-00-6
Molecular Formula:C₃₀H₃₅N₃O₆
Molecular Weight:533.624
Hs Code.:

Synonyms:(R)-allyl 4-(9,9-dimethyl-5-(naphthalen-2-ylmethyl)-(4,7-dioxo-2,8-dioxa-3,6-diazadecyl))benzylcarbamate

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Chemical Property of (R)-allyl 4-(9,9-dimethyl-5-(naphthalen-2-ylmethyl)-(4,7-dioxo-2,8-dioxa-3,6-diazadecyl))benzylcarbamate

Chemical Property:

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Technology Process of (R)-allyl 4-(9,9-dimethyl-5-(naphthalen-2-ylmethyl)-(4,7-dioxo-2,8-dioxa-3,6-diazadecyl))benzylcarbamate

There total 6 articles about (R)-allyl 4-(9,9-dimethyl-5-(naphthalen-2-ylmethyl)-(4,7-dioxo-2,8-dioxa-3,6-diazadecyl))benzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.8%

: 1173159-00-6
(R)-allyl 4-(9,9-dimethyl-5-(naphthalen-2-ylmethyl)-(4,7-dioxo-2,8-dioxa-3,6-diazadecyl))benzylcarbamate

Guidance literature:

Reference yield:

: 1173158-95-6
N-({4-[(aminooxy)methyl]phenyl}methyl)prop-2-enyloxycarboxamide

: 76985-10-9
Boc-D-2Nal-OH

: 1173159-00-6
(R)-allyl 4-(9,9-dimethyl-5-(naphthalen-2-ylmethyl)-(4,7-dioxo-2,8-dioxa-3,6-diazadecyl))benzylcarbamate

Guidance literature:: With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 22 ℃;

Reference yield:

: 1007859-08-6
N-((4-(hydroxymethyl)phenyl)methyl)prop-2-enyloxycarboxamide

: 1173159-00-6
(R)-allyl 4-(9,9-dimethyl-5-(naphthalen-2-ylmethyl)-(4,7-dioxo-2,8-dioxa-3,6-diazadecyl))benzylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,1'-azodicarbonyl-dipiperidine; triphenylphosphine / tetrahydrofuran / 23 h / 20 °C / Inert atmosphere

1.2: 5 h / 50 °C

2.1: hydrazine hydrate / methanol / 0.5 h / Reflux

3.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 22 °C

With hydrazine hydrate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;