(2R,3S)-methyl 3-(2-nitrophenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

Base Information

Chemical Name:(2R,3S)-methyl 3-(2-nitrophenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate
CAS No.:960215-89-8
Molecular Formula:C₁₆H₁₆N₂O₅
Molecular Weight:316.313
Hs Code.:

Synonyms:(2R,3S)-methyl 3-(2-nitrophenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-methyl 3-(2-nitrophenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

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Technology Process of (2R,3S)-methyl 3-(2-nitrophenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

There total 1 articles about (2R,3S)-methyl 3-(2-nitrophenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 96243-73-1
(1R,2S,3R,4S)-3-(methoxycarbonyl)bicyclo[2.2.1]hept-5-ene-2-carboxylic acid

: 88-74-4
2-nitro-aniline

: 960215-89-8
(2R,3S)-methyl 3-(2-nitrophenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.tetasy.2007.09.019

Reference yield:

: 960215-89-8
(2R,3S)-methyl 3-(2-nitrophenylcarbamoyl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

: ((2R,3S)-3-((2-aminophenylamino)methyl)bicyclo[2.2.1]heptan-2-yl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 24 h / Heating

2: 0.67 g / H₂ / Pd/C / CH₂Cl₂ / 20 °C

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; dichloromethane;
DOI:10.1016/j.tetasy.2007.09.019