C₄₂H₅₂N₆O₈

Base Information

Chemical Name:C₄₂H₅₂N₆O₈
CAS No.:1357008-17-3
Molecular Formula:C₄₂H₅₂N₆O₈
Molecular Weight:768.91
Hs Code.:

C<sub>42</sub>H<sub>52</sub>N<sub>6</sub>O<sub>8</sub>

Synonyms:C₄₂H₅₂N₆O₈

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Chemical Property of C₄₂H₅₂N₆O₈

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Technology Process of C₄₂H₅₂N₆O₈

There total 13 articles about C₄₂H₅₂N₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₇H₆₀N₆O₁₀

: 1357008-17-3
C₄₂H₅₂N₆O₈

Guidance literature:: With methoxybenzene; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.tet.2011.11.089

Reference yield:

: 1357008-12-8
C₂₂H₃₄N₂O₆

: 1357008-17-3
C₄₂H₅₂N₆O₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogen; palladium / ethanol

2.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.33 h / -47 °C / Inert atmosphere

3.2: -47 - 20 °C

4.1: methoxybenzene; trifluoroacetic acid / dichloromethane

5.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 1 h / 20 °C / Inert atmosphere

6.1: dihydrogen peroxide; lithium hydroxide / methanol / 0 °C

6.2: pH 1

7.1: methoxybenzene; trifluoroacetic acid / dichloromethane

With diethylamino-sulfur trifluoride; hydrogen; dihydrogen peroxide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; palladium; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; lithium hydroxide; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.tet.2011.11.089

Reference yield:

: 1357008-14-0
C₃₉H₅₀N₄O₈

: 1357008-17-3
C₄₂H₅₂N₆O₈

Guidance literature:: Multi-step reaction with 3 steps

1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: dihydrogen peroxide; lithium hydroxide / methanol / 0 °C

2.2: pH 1

3.1: methoxybenzene; trifluoroacetic acid / dichloromethane

With dihydrogen peroxide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; lithium hydroxide; In methanol; dichloromethane;
DOI:10.1016/j.tet.2011.11.089