10-benzyl-7,8-dimethoxy-2,3,4,10-tetrahydropyrido<2',3':4,5>imidazo<1,2-a>pyrimidine

Base Information

Chemical Name:10-benzyl-7,8-dimethoxy-2,3,4,10-tetrahydropyrido<2',3':4,5>imidazo<1,2-a>pyrimidine
CAS No.:128278-35-3
Molecular Formula:C₁₈H₂₀N₄O₂
Molecular Weight:324.382
Hs Code.:

Synonyms:10-benzyl-7,8-dimethoxy-2,3,4,10-tetrahydropyrido<2',3':4,5>imidazo<1,2-a>pyrimidine

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Chemical Property of 10-benzyl-7,8-dimethoxy-2,3,4,10-tetrahydropyrido<2',3':4,5>imidazo<1,2-a>pyrimidine

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Technology Process of 10-benzyl-7,8-dimethoxy-2,3,4,10-tetrahydropyrido<2',3':4,5>imidazo<1,2-a>pyrimidine

There total 4 articles about 10-benzyl-7,8-dimethoxy-2,3,4,10-tetrahydropyrido<2',3':4,5>imidazo<1,2-a>pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 128278-12-6
10-benzyl-7,8-dimethoxy-2,3,4,10-tetrahydropyrido<2',3':4,5>imidazo<1,2-a>pyrimidin-2-one

: 128278-35-3
10-benzyl-7,8-dimethoxy-2,3,4,10-tetrahydropyrido<2',3':4,5>imidazo<1,2-a>pyrimidine

Guidance literature:: With diborane; In tetrahydrofuran; for 1.25h; Heating;

Reference yield:

: 128278-10-4
2-benzylamino-5,6-dimethoxy-3-nitropyridine

: 128278-35-3
10-benzyl-7,8-dimethoxy-2,3,4,10-tetrahydropyrido<2',3':4,5>imidazo<1,2-a>pyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Raney Ni / tetrahydrofuran / 60 °C

2: NEt₃ / 0.5 h

3: 74 percent / dimethylformamide / 2 h / Heating

4: 82 percent / 2M B₂H₆ / tetrahydrofuran / 1.25 h / Heating

With hydrogen; triethylamine; diborane; nickel; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: N²-Benzyl-5,6-dimethoxy-pyridine-2,3-diamine

: 128278-35-3
10-benzyl-7,8-dimethoxy-2,3,4,10-tetrahydropyrido<2',3':4,5>imidazo<1,2-a>pyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: NEt₃ / 0.5 h

2: 74 percent / dimethylformamide / 2 h / Heating

3: 82 percent / 2M B₂H₆ / tetrahydrofuran / 1.25 h / Heating

With triethylamine; diborane; In tetrahydrofuran; N,N-dimethyl-formamide;