t-butyl {2-[2-benzylamino-5-(4-fluoro-benzylsulfamoyl)phenylcarbamoyl]-ethyl}carbamate

Base Information

Chemical Name:t-butyl {2-[2-benzylamino-5-(4-fluoro-benzylsulfamoyl)phenylcarbamoyl]-ethyl}carbamate
CAS No.:845833-88-7
Molecular Formula:C₂₈H₃₃FN₄O₅S
Molecular Weight:556.658
Hs Code.:

Synonyms:t-butyl {2-[2-benzylamino-5-(4-fluoro-benzylsulfamoyl)phenylcarbamoyl]-ethyl}carbamate

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Chemical Property of t-butyl {2-[2-benzylamino-5-(4-fluoro-benzylsulfamoyl)phenylcarbamoyl]-ethyl}carbamate

Chemical Property:

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Technology Process of t-butyl {2-[2-benzylamino-5-(4-fluoro-benzylsulfamoyl)phenylcarbamoyl]-ethyl}carbamate

There total 1 articles about t-butyl {2-[2-benzylamino-5-(4-fluoro-benzylsulfamoyl)phenylcarbamoyl]-ethyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3303-84-2
3-(tert-butyloxycarbonylamino)propionic acid

: 845833-87-6
3-amino-4-benzylamino-N-(4-fluoro-benzyl)-benzenesulfonamide

: 845833-88-7
t-butyl {2-[2-benzylamino-5-(4-fluoro-benzylsulfamoyl)phenylcarbamoyl]-ethyl}carbamate

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.bmcl.2004.10.090

Reference yield:

: 845833-88-7
t-butyl {2-[2-benzylamino-5-(4-fluoro-benzylsulfamoyl)phenylcarbamoyl]-ethyl}carbamate

: 1-benzyl-2-[2-(3-ethyl-ureido)-ethyl]-1H-benzoimidazole-5-sulfonic acid 4-fluoro-benzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: AcOH / 3 h / 90 °C

2: HCl / CH₂Cl₂; dioxane / 20 °C

3: triethylamine / CH₂Cl₂ / 20 °C

With hydrogenchloride; acetic acid; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2004.10.090

Reference yield:

: 845833-88-7
t-butyl {2-[2-benzylamino-5-(4-fluoro-benzylsulfamoyl)phenylcarbamoyl]-ethyl}carbamate

: 1-benzyl-2-[2-(3-isopropyl-ureido)ethyl]-1H-benzimidazole-5-(4-fluorobenzyl)sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: AcOH / 3 h / 90 °C

2: HCl / CH₂Cl₂; dioxane / 20 °C

3: triethylamine / CH₂Cl₂ / 20 °C

With hydrogenchloride; acetic acid; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2004.10.090