(R)-benzyl 1-(benzo[d][1,3]dioxol-5-yl)-2-hydroxyethylcarbamate

Base Information

• Chemical Name: (R)-benzyl 1-(benzo[d][1,3]dioxol-5-yl)-2-hydroxyethylcarbamate
• CAS No.: 1080596-31-1
• Molecular Formula: C₁₇H₁₇NO₅
• Molecular Weight: 315.326
• Mol file: 1080596-31-1.mol

Synonyms:(R)-benzyl 1-(benzo[d][1,3]dioxol-5-yl)-2-hydroxyethylcarbamate

Chemical Property of (R)-benzyl 1-(benzo[d][1,3]dioxol-5-yl)-2-hydroxyethylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (R)-benzyl 1-(benzo[d][1,3]dioxol-5-yl)-2-hydroxyethylcarbamate

There total 1 articles about (R)-benzyl 1-(benzo[d][1,3]dioxol-5-yl)-2-hydroxyethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

5-vinyl-1,3-benzodioxole (7315-32-4) + O-benzyl carbamate (621-84-1) → (R)-benzyl 1-(benzo[d][1,3]dioxol-5-yl)-2-hydroxyethylcarbamate (1080596-31-1)

Guidance literature:

O-benzyl carbamate; With tert-butylhypochlorite; 1,4-bis(9-O-dihydroquinidine)phthalazine; In propan-1-ol; water; at 0 ℃; for 0.166667h;

5-vinyl-1,3-benzodioxole; With potassium osmate; sodium hydroxide; In propan-1-ol; water; at 0 ℃; for 4.5h; optical yield given as %ee;

DOI:10.1021/jo801721z

Reference yield:

(R)-benzyl 1-(benzo[d][1,3]dioxol-5-yl)-2-hydroxyethylcarbamate (1080596-31-1) → C9H11NO3

Guidance literature:

With palladium on carbon; ammonium acetate; hydrogen; In methanol; at 20 ℃; for 21h; under 760.051 Torr;

DOI:10.1021/jo801721z

upstream raw materials:

5-vinyl-1,3-benzodioxole

O-benzyl carbamate