(2R,4'R,5'R,2''E)-3-benzyloxy-2-benzyloxycarbonylamino-2-(5'-[9''-(2'''-hexyl-[1''',3''']dioxolan-2'''-yl)non-2''-enyl]-2',2'-dimethyl-[1',3']dioxolan-4'-yl)-propionicacid 8-phenylmenthyl ester

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Chemical Name:(2R,4'R,5'R,2''E)-3-benzyloxy-2-benzyloxycarbonylamino-2-(5'-[9''-(2'''-hexyl-[1''',3''']dioxolan-2'''-yl)non-2''-enyl]-2',2'-dimethyl-[1',3']dioxolan-4'-yl)-propionicacid 8-phenylmenthyl ester
CAS No.:1059067-76-3
Molecular Formula:C₅₇H₈₁NO₉
Molecular Weight:924.271
Hs Code.:

(2R,4'R,5'R,2''E)-3-benzyloxy-2-benzyloxycarbonylamino-2-(5'-[9''-(2'''-hexyl-[1''',3''']dioxolan-2'''-yl)non-2''-enyl]-2',2'-dimethyl-[1',3']dioxolan-4'-yl)-propionicacid 8-phenylmenthyl ester

Synonyms:(2R,4'R,5'R,2''E)-3-benzyloxy-2-benzyloxycarbonylamino-2-(5'-[9''-(2'''-hexyl-[1''',3''']dioxolan-2'''-yl)non-2''-enyl]-2',2'-dimethyl-[1',3']dioxolan-4'-yl)-propionicacid 8-phenylmenthyl ester

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Chemical Property of (2R,4'R,5'R,2''E)-3-benzyloxy-2-benzyloxycarbonylamino-2-(5'-[9''-(2'''-hexyl-[1''',3''']dioxolan-2'''-yl)non-2''-enyl]-2',2'-dimethyl-[1',3']dioxolan-4'-yl)-propionicacid 8-phenylmenthyl ester

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Technology Process of (2R,4'R,5'R,2''E)-3-benzyloxy-2-benzyloxycarbonylamino-2-(5'-[9''-(2'''-hexyl-[1''',3''']dioxolan-2'''-yl)non-2''-enyl]-2',2'-dimethyl-[1',3']dioxolan-4'-yl)-propionicacid 8-phenylmenthyl ester

There total 1 articles about (2R,4'R,5'R,2''E)-3-benzyloxy-2-benzyloxycarbonylamino-2-(5'-[9''-(2'''-hexyl-[1''',3''']dioxolan-2'''-yl)non-2''-enyl]-2',2'-dimethyl-[1',3']dioxolan-4'-yl)-propionicacid 8-phenylmenthyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1059067-75-2
(2R,4'R,5'R)-3-benzyloxy-2-benzyloxycarbonylamino-2-(2',2'-dimethyl-5'-[2''-(1-phenyl-1H-tetrazol-5-sulfonyl)ethyl]-[1',3']dioxolan-4'-yl)propionic acid 8-phenylmenthyl ester

: 172330-97-1
7-(2-hexyl-1,3-dioxolan-2-yl)heptanal

: 1059067-76-3
(2R,4'R,5'R,2''E)-3-benzyloxy-2-benzyloxycarbonylamino-2-(5'-[9''-(2'''-hexyl-[1''',3''']dioxolan-2'''-yl)non-2''-enyl]-2',2'-dimethyl-[1',3']dioxolan-4'-yl)-propionicacid 8-phenylmenthyl ester

Guidance literature:: (2R,4'R,5'R)-3-benzyloxy-2-benzyloxycarbonylamino-2-(2',2'-dimethyl-5'-[2''-(1-phenyl-1H-tetrazol-5-sulfonyl)ethyl]-[1',3']dioxolan-4'-yl)propionic acid 8-phenylmenthyl ester; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h;

7-(2-hexyl-1,3-dioxolan-2-yl)heptanal; In tetrahydrofuran; at -78 - 20 ℃; stereoselective reaction;
DOI:10.1021/ol801709c