C₃₈H₆₈O₇SSi₃

Base Information

Chemical Name:C₃₈H₆₈O₇SSi₃
CAS No.:236427-75-1
Molecular Formula:C₃₈H₆₈O₇SSi₃
Molecular Weight:753.276
Hs Code.:

C<sub>38</sub>H<sub>68</sub>O<sub>7</sub>SSi<sub>3</sub>

Synonyms:C₃₈H₆₈O₇SSi₃

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Chemical Property of C₃₈H₆₈O₇SSi₃

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Technology Process of C₃₈H₆₈O₇SSi₃

There total 17 articles about C₃₈H₆₈O₇SSi₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 236427-74-0
C₃₈H₆₈O₅SSi₃

: 236427-75-1
C₃₈H₆₈O₇SSi₃

Guidance literature:: With sodium dihydrogenphosphate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 0.416667h; Ambient temperature;
DOI:10.1055/s-1999-2689

Reference yield:

: 4039-82-1
Benzyl propargyl ether

: 236427-75-1
C₃₈H₆₈O₇SSi₃

Guidance literature:: Multi-step reaction with 16 steps

1: 88 percent / BuLi / tetrahydrofuran / 0.83 h / -78 - 0 °C

2: 73 percent / LAH / tetrahydrofuran / 7.5 h / -78 - 0 °C

3: 93 percent / L-(+)-DET, TBHP, Ti(O-i-Pr)4, molecular sieves 4 Angstroem / CH₂Cl₂ / 21 h / -25 °C

4: 94 percent / Ti(O-i-Pr)4 / CH₂Cl₂ / 2 h / Ambient temperature

5: 94 percent / NaOH, H₂O / methanol / 0.75 h / Ambient temperature

6: 76 percent / pyridine / CH₂Cl₂ / 18 h / 0 °C

7: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0.42 h / 0 °C

8: 98 percent / DIBAL / CH₂Cl₂ / 0.33 h / -78 °C

9: Dess-Martin periodinane / CH₂Cl₂ / 48 h

10: benzene / 21 h / Ambient temperature

11: 99 percent / DIBAL / CH₂Cl₂ / 0.33 h / -78 °C

12: 93 percent / D-(-)-DET, TBHP, Ti(O-i-Pr)4, molecular sieves 4 Angstroem / CH₂Cl₂ / 21 h / -25 °C

13: 96 percent / diethyl ether / 23 h / -30 °C

14: 76 percent / Bu₃P / CH₂Cl₂ / 4 h / Ambient temperature

15: 100 percent / (i-Pr)2NEt, TBAI / 1,2-dichloro-ethane / 6 h / Heating

16: 95 percent / m-CPBA, NaH₂PO₄ / CH₂Cl₂ / 0.42 h / Ambient temperature

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hydroxide; sodium dihydrogenphosphate; lithium aluminium tetrahydride; n-butyllithium; diethyl (2S,3S)-tartrate; diethyl (2R,3R)-tartrate; tributylphosphine; 4 A molecular sieve; water; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 1,2-dichloro-ethane; benzene;
DOI:10.1055/s-1999-2689

Reference yield:

: 80885-30-9,81028-03-7,69152-88-1
(E)-4-(benzyloxy)-2-buten-1-ol

: 236427-75-1
C₃₈H₆₈O₇SSi₃

Guidance literature:: Multi-step reaction with 14 steps

1: 93 percent / L-(+)-DET, TBHP, Ti(O-i-Pr)4, molecular sieves 4 Angstroem / CH₂Cl₂ / 21 h / -25 °C

2: 94 percent / Ti(O-i-Pr)4 / CH₂Cl₂ / 2 h / Ambient temperature

3: 94 percent / NaOH, H₂O / methanol / 0.75 h / Ambient temperature

4: 76 percent / pyridine / CH₂Cl₂ / 18 h / 0 °C

5: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0.42 h / 0 °C

6: 98 percent / DIBAL / CH₂Cl₂ / 0.33 h / -78 °C

7: Dess-Martin periodinane / CH₂Cl₂ / 48 h

8: benzene / 21 h / Ambient temperature

9: 99 percent / DIBAL / CH₂Cl₂ / 0.33 h / -78 °C

10: 93 percent / D-(-)-DET, TBHP, Ti(O-i-Pr)4, molecular sieves 4 Angstroem / CH₂Cl₂ / 21 h / -25 °C

11: 96 percent / diethyl ether / 23 h / -30 °C

12: 76 percent / Bu₃P / CH₂Cl₂ / 4 h / Ambient temperature

13: 100 percent / (i-Pr)2NEt, TBAI / 1,2-dichloro-ethane / 6 h / Heating

14: 95 percent / m-CPBA, NaH₂PO₄ / CH₂Cl₂ / 0.42 h / Ambient temperature

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hydroxide; sodium dihydrogenphosphate; diethyl (2S,3S)-tartrate; diethyl (2R,3R)-tartrate; tributylphosphine; 4 A molecular sieve; water; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether; dichloromethane; 1,2-dichloro-ethane; benzene;
DOI:10.1055/s-1999-2689