benzyl N-bis(4-methoxyphenyl)methylene-O-[O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl]-L-serinate

Base Information

• Chemical Name: benzyl N-bis(4-methoxyphenyl)methylene-O-[O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl]-L-serinate
• CAS No.: 936115-47-8
• Molecular Formula: C₅₁H₅₉NO₂₂
• Molecular Weight: 1038.02
• Mol file: 936115-47-8.mol

Synonyms:benzyl N-bis(4-methoxyphenyl)methylene-O-[O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl]-L-serinate

Chemical Property of benzyl N-bis(4-methoxyphenyl)methylene-O-[O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl]-L-serinate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl N-bis(4-methoxyphenyl)methylene-O-[O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl]-L-serinate

There total 12 articles about benzyl N-bis(4-methoxyphenyl)methylene-O-[O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl]-L-serinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

benzyl N-bis(4-methoxyphenyl)methylene-L-serinate (936115-45-6) + lactose octaacetate (3616-19-1,5328-50-7,5346-90-7,6291-42-5,6920-00-9,20764-63-0,20880-60-8,20880-65-3,22352-19-8,23973-20-8,32447-69-1,34213-32-6,53956-64-2,56907-29-0,56994-12-8,56994-13-9,57128-38-8,67650-36-6,68036-17-9,68036-19-1,78215-50-6,78215-51-7,79549-48-7,80446-82-8,85249-04-3,93221-83-1,93779-27-2,111407-83-1,111407-84-2,111407-85-3,120328-65-6,123809-59-6,132341-46-9,132341-47-0,132341-49-2,145307-94-4,52554-32-2) → benzyl N-bis(4-methoxyphenyl)methylene-O-[O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl]-L-serinate (936115-47-8)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃;

DOI:10.1080/07328303.2010.508295

Reference yield: 69.0%

→ benzyl N-bis(4-methoxyphenyl)methylene-O-[O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl]-L-serinate (936115-47-8)

Guidance literature:

Reference yield:

C25H25NO5 (1253053-57-4) + 1',2',3',6',2,3,4,6-octa-O-acetyl-β-D-lactose (3616-19-1,5328-50-7,5346-90-7,6291-42-5,6920-00-9,20764-63-0,20880-60-8,20880-65-3,22352-19-8,23973-20-8,32447-69-1,34213-32-6,52554-32-2,53956-64-2,56907-29-0,56994-12-8,56994-13-9,57128-38-8,67650-36-6,68036-17-9,68036-19-1,78215-50-6,78215-51-7,79549-48-7,80446-82-8,85249-04-3,93221-83-1,93779-27-2,111407-83-1,111407-84-2,111407-85-3,120328-65-6,123809-59-6,132341-46-9,132341-47-0,132341-49-2,145307-94-4) → benzyl N-bis(4-methoxyphenyl)methylene-O-[O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl]-L-serinate (936115-47-8) + C51H59NO22 (1253053-77-8)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 48h; optical yield given as %de;

DOI:10.1080/07328303.2010.508295

upstream raw materials:

1-bromo-4-methoxy-benzene

C₂₅H₂₅NO₅

1',2',3',6',2,3,4,6-octa-O-acetyl-β-D-lactose

benzyl N-bis(4-methoxyphenyl)methylene-L-serinate