(1R)-(1,3,4/2,6)-1-O-benzoyl-2,3-O-cyclohexylidene-4-<(benzyloxycarbonyl)amino>-6-C-(bromomethyl)-1,2,3-cyclohexanetriol

Base Information

Chemical Name:(1R)-(1,3,4/2,6)-1-O-benzoyl-2,3-O-cyclohexylidene-4-<(benzyloxycarbonyl)amino>-6-C-(bromomethyl)-1,2,3-cyclohexanetriol
CAS No.:89859-87-0
Molecular Formula:C₂₈H₃₂BrNO₆
Molecular Weight:558.469
Hs Code.:

Synonyms:(1R)-(1,3,4/2,6)-1-O-benzoyl-2,3-O-cyclohexylidene-4-<(benzyloxycarbonyl)amino>-6-C-(bromomethyl)-1,2,3-cyclohexanetriol

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Chemical Property of (1R)-(1,3,4/2,6)-1-O-benzoyl-2,3-O-cyclohexylidene-4-<(benzyloxycarbonyl)amino>-6-C-(bromomethyl)-1,2,3-cyclohexanetriol

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Technology Process of (1R)-(1,3,4/2,6)-1-O-benzoyl-2,3-O-cyclohexylidene-4-<(benzyloxycarbonyl)amino>-6-C-(bromomethyl)-1,2,3-cyclohexanetriol

There total 3 articles about (1R)-(1,3,4/2,6)-1-O-benzoyl-2,3-O-cyclohexylidene-4-<(benzyloxycarbonyl)amino>-6-C-(bromomethyl)-1,2,3-cyclohexanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 89859-87-0
(1R)-(1,3,4/2,6)-1-O-benzoyl-2,3-O-cyclohexylidene-4-<(benzyloxycarbonyl)amino>-6-C-(bromomethyl)-1,2,3-cyclohexanetriol

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / p-toluenosulfonic acid / dimethylformamide / 1 h / 60 - 65 °C / 60 Torr

2: 59 percent / N-bromosuccinimide, BaCO₃ / CCl₄; various solvent(s) / 1 h / Heating

3: 95 percent / p-toluenesulfonic acid / dimethylformamide / 2 h / 55 °C / 40 Torr

With N-Bromosuccinimide; toluene-4-sulfonic acid; barium carbonate; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00156a023

Reference yield:

: 85281-05-6
N-(benzyloxycarbonyl)validamine

: 89859-87-0
(1R)-(1,3,4/2,6)-1-O-benzoyl-2,3-O-cyclohexylidene-4-<(benzyloxycarbonyl)amino>-6-C-(bromomethyl)-1,2,3-cyclohexanetriol

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / p-toluenosulfonic acid / dimethylformamide / 1 h / 60 - 65 °C / 60 Torr

2: 59 percent / N-bromosuccinimide, BaCO₃ / CCl₄; various solvent(s) / 1 h / Heating

3: 95 percent / p-toluenesulfonic acid / dimethylformamide / 2 h / 55 °C / 40 Torr

With N-Bromosuccinimide; toluene-4-sulfonic acid; barium carbonate; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00156a023

Reference yield:

: 89859-47-2
(1R)-(1,3,4/2,6)-1,7-O-benzylidene-4-<(benzyloxycarbonyl)amino>-6-C-(hydroxymethyl)-1,2,3-cyclohexanetriol

: 89859-87-0
(1R)-(1,3,4/2,6)-1-O-benzoyl-2,3-O-cyclohexylidene-4-<(benzyloxycarbonyl)amino>-6-C-(bromomethyl)-1,2,3-cyclohexanetriol

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / N-bromosuccinimide, BaCO₃ / CCl₄; various solvent(s) / 1 h / Heating

2: 95 percent / p-toluenesulfonic acid / dimethylformamide / 2 h / 55 °C / 40 Torr

With N-Bromosuccinimide; toluene-4-sulfonic acid; barium carbonate; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00156a023