methyl 9-phenyl-2(E)-nonenoate

Base Information

Chemical Name:methyl 9-phenyl-2(E)-nonenoate
CAS No.:260050-22-4
Molecular Formula:C₁₆H₂₂O₂
Molecular Weight:246.349
Hs Code.:

Synonyms:methyl 9-phenyl-2(E)-nonenoate

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Chemical Property of methyl 9-phenyl-2(E)-nonenoate

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Technology Process of methyl 9-phenyl-2(E)-nonenoate

There total 6 articles about methyl 9-phenyl-2(E)-nonenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.3%

: 1067-74-9
Methyl diethylphosphonoacetate

: 121784-15-4
7-phenylheptanal

: 260050-22-4
methyl 9-phenyl-2(E)-nonenoate

Guidance literature:: Methyl diethylphosphonoacetate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

7-phenylheptanal; In tetrahydrofuran; at 0 ℃; for 0.25h;
DOI:10.1016/S0968-0896(99)00253-9

Reference yield:

: 10521-91-2
5-phenylpentan-1-ol

: 260050-22-4
methyl 9-phenyl-2(E)-nonenoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: 100 percent / oxalyl chloride; DMSO / CH₂Cl₂ / 0.25 h / -55 °C

2.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

2.2: 86 percent / tetrahydrofuran / 0.25 h / 0 °C

3.1: 91 percent / H₂ / Pd/C / methanol / 7500.6 Torr

4.1: 77 percent / DIBALH / CH₂Cl₂ / 0.5 h / -75 °C

5.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

5.2: 79.3 percent / tetrahydrofuran / 0.25 h / 0 °C

With oxalyl dichloride; hydrogen; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; 1.1: Oxidation / 2.1: deprotonation / 2.2: Condensation / 3.1: Hydrogenation / 4.1: Reduction / 5.1: deprotonation / 5.2: Condensation;
DOI:10.1016/S0968-0896(99)00253-9

Reference yield:

: 2270-20-4
5-Phenylpentanoic acid

: 260050-22-4
methyl 9-phenyl-2(E)-nonenoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: 100 percent / LiAlH₄ / diethyl ether / 0 - 20 °C

2.1: 100 percent / oxalyl chloride; DMSO / CH₂Cl₂ / 0.25 h / -55 °C

3.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

3.2: 86 percent / tetrahydrofuran / 0.25 h / 0 °C

4.1: 91 percent / H₂ / Pd/C / methanol / 7500.6 Torr

5.1: 77 percent / DIBALH / CH₂Cl₂ / 0.5 h / -75 °C

6.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

6.2: 79.3 percent / tetrahydrofuran / 0.25 h / 0 °C

With lithium aluminium tetrahydride; oxalyl dichloride; hydrogen; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 1.1: Reduction / 2.1: Oxidation / 3.1: deprotonation / 3.2: Condensation / 4.1: Hydrogenation / 5.1: Reduction / 6.1: deprotonation / 6.2: Condensation;
DOI:10.1016/S0968-0896(99)00253-9