Technology Process of C22H22O5
There total 7 articles about C22H22O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
tetrahydrofuran;
at 80 ℃;
Inert atmosphere;
DOI:10.1021/ja203642n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sulfuric acid / 0 - 20 °C / Inert atmosphere
2: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere
With
sulfuric acid; toluene-4-sulfonic acid;
In
tetrahydrofuran;
DOI:10.1021/ja203642n
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere
1.2: 0 - 45 °C / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere
3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C
4.1: sodium chlorite; sodium phosphate monobasic monohydrate / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0 °C
5.1: sulfuric acid / 0 - 20 °C / Inert atmosphere
6.1: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere
With
sodium chlorite; sodium phosphate monobasic monohydrate; sulfuric acid; tetrabutyl ammonium fluoride; sodium hydride; toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; 2-methyl-but-2-ene; water; ethyl acetate; mineral oil; tert-butyl alcohol;
4.1: Pinnick oxidation;
DOI:10.1021/ja203642n
