Technology Process of C18H29(2)HO7Si
There total 18 articles about C18H29(2)HO7Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 99 percent / methanol; diethyl ether / 15 h / Ambient temperature
2: 90 percent / p-toluenesulfonic acid, Na2CO3 / CH2Cl2 / 5 °C
3: imidazole / dimethylformamide / 1.75 h
4: 1.) H2O, AcOH; 2) pyridinium dichromate / 1.) methanol, toluene r.t., 1 h; 2.) DMF, 45 deg C, 1 h
6: sodium borodeuteride / ethanol / 0.17 h / 5 °C
With
1H-imidazole; dipyridinium dichromate; sodium borodeuteride; water; sodium carbonate; toluene-4-sulfonic acid; acetic acid;
In
methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / p-toluenesulfonic acid, Na2CO3 / CH2Cl2 / 5 °C
2: imidazole / dimethylformamide / 1.75 h
3: 1.) H2O, AcOH; 2) pyridinium dichromate / 1.) methanol, toluene r.t., 1 h; 2.) DMF, 45 deg C, 1 h
5: sodium borodeuteride / ethanol / 0.17 h / 5 °C
With
1H-imidazole; dipyridinium dichromate; sodium borodeuteride; water; sodium carbonate; toluene-4-sulfonic acid; acetic acid;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: imidazole / dimethylformamide / 1.75 h
2: 1.) H2O, AcOH; 2) pyridinium dichromate / 1.) methanol, toluene r.t., 1 h; 2.) DMF, 45 deg C, 1 h
4: sodium borodeuteride / ethanol / 0.17 h / 5 °C
With
1H-imidazole; dipyridinium dichromate; sodium borodeuteride; water; acetic acid;
In
ethanol; N,N-dimethyl-formamide;