p-Nitrobenzyl trichloromethanesulfinate

Base Information

Chemical Name:p-Nitrobenzyl trichloromethanesulfinate
CAS No.:55613-67-7
Molecular Formula:C₈H₆Cl₃NO₄S
Molecular Weight:318.565
Hs Code.:

Synonyms:p-Nitrobenzyl trichloromethanesulfinate

Suppliers and Price of p-Nitrobenzyl trichloromethanesulfinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-Nitrobenzyl trichloromethanesulfinate

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Technology Process of p-Nitrobenzyl trichloromethanesulfinate

There total 3 articles about p-Nitrobenzyl trichloromethanesulfinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 55613-68-8
p-Nitrobenzyl trichloromethanesulfenate

: 55613-67-7
p-Nitrobenzyl trichloromethanesulfinate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1.) 90 min, 0 deg C, 2.) 120 min, 25 deg C;
DOI:10.1016/S0040-4020(01)88389-7

Reference yield:

: 619-73-8
4-nitrobenzyl chloride

: 55613-67-7
p-Nitrobenzyl trichloromethanesulfinate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / 72 h / Ambient temperature

2: 90 percent / 80percent MCPBA / CH₂Cl₂ / 1.) 90 min, 0 deg C, 2.) 120 min, 25 deg C

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4020(01)88389-7