(Z)-8-O-benzoyl-2,3,4-trideoxy-6,7-O-isopropylidene-D-arabino-oct-3-enose propane-1,3-diyl acetal

Base Information

Chemical Name:(Z)-8-O-benzoyl-2,3,4-trideoxy-6,7-O-isopropylidene-D-arabino-oct-3-enose propane-1,3-diyl acetal
CAS No.:136933-11-4
Molecular Formula:C₂₁H₂₈O₇
Molecular Weight:392.449
Hs Code.:

Synonyms:(Z)-8-O-benzoyl-2,3,4-trideoxy-6,7-O-isopropylidene-D-arabino-oct-3-enose propane-1,3-diyl acetal

Suppliers and Price of (Z)-8-O-benzoyl-2,3,4-trideoxy-6,7-O-isopropylidene-D-arabino-oct-3-enose propane-1,3-diyl acetal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-8-O-benzoyl-2,3,4-trideoxy-6,7-O-isopropylidene-D-arabino-oct-3-enose propane-1,3-diyl acetal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-8-O-benzoyl-2,3,4-trideoxy-6,7-O-isopropylidene-D-arabino-oct-3-enose propane-1,3-diyl acetal

There total 4 articles about (Z)-8-O-benzoyl-2,3,4-trideoxy-6,7-O-isopropylidene-D-arabino-oct-3-enose propane-1,3-diyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 613-90-1
benzoyl cyanide

: 136933-07-8,136933-08-9
(E/Z)-2,3,4-trideoxy-6,7-O-isopropylidene-D-arabino-oct-3-enose propane-1,3-diyl acetal

: 136933-11-4
(Z)-8-O-benzoyl-2,3,4-trideoxy-6,7-O-isopropylidene-D-arabino-oct-3-enose propane-1,3-diyl acetal

Guidance literature:: In acetonitrile; at -20 ℃; for 2h;
DOI:10.1016/0008-6215(92)84183-S

Reference yield:

: 69891-92-5
2-(1,3-dioxan-2-yl)ethyltriphenylphosphonium bromide

: 136933-11-4
(Z)-8-O-benzoyl-2,3,4-trideoxy-6,7-O-isopropylidene-D-arabino-oct-3-enose propane-1,3-diyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1) KOtBu / 1) THF, r.t., 30 min, 2) 10 min

2: 94 percent / acetonitrile / 2 h / -20 °C

With potassium tert-butylate; In acetonitrile;
DOI:10.1016/0008-6215(92)84183-S

Reference yield:

: 58645-35-5,58645-40-2,144216-75-1
3,4-O-isopropylidene-D-arabinopyranose

: 136933-11-4
(Z)-8-O-benzoyl-2,3,4-trideoxy-6,7-O-isopropylidene-D-arabino-oct-3-enose propane-1,3-diyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1) KOtBu / 1) THF, r.t., 30 min, 2) 10 min

2: 94 percent / acetonitrile / 2 h / -20 °C

With potassium tert-butylate; In acetonitrile;
DOI:10.1016/0008-6215(92)84183-S