(2'S,3'S,4'S,5'R,6'R)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone

Base Information

• Chemical Name: (2'S,3'S,4'S,5'R,6'R)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone
• CAS No.: 138512-04-6
• Molecular Formula: C₃₂H₂₉IO₁₁
• Molecular Weight: 716.48

Synonyms:(2'S,3'S,4'S,5'R,6'R)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone

Chemical Property of (2'S,3'S,4'S,5'R,6'R)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone

Chemical Property:

Purity/Quality:

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Technology Process of (2'S,3'S,4'S,5'R,6'R)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone

There total 5 articles about (2'S,3'S,4'S,5'R,6'R)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone (138407-83-7,138512-18-2) → (2'R,3'R,4'R,5'S,6'S)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone (138407-78-0) + (2'R,3'S,4'R,5'S,6'S)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone (138407-78-0,138512-04-6) + (2'S,3'S,4'R,5'S,6'S)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone (138407-78-0,138512-04-6)

Guidance literature:

With pyridine; hydrogen fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 11h; Yield given. Yields of byproduct given;

Reference yield:

7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone (138407-83-7,138512-18-2) → (2'R,3'R,4'R,5'S,6'S)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone (138407-78-0) + (2'R,3'S,4'R,5'S,6'S)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone (138407-78-0,138512-04-6) + (2'S,3'S,4'R,5'S,6'S)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone (138407-78-0,138512-04-6)

Guidance literature:

With pyridine; hydrogen fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 11h; Yield given. Yields of byproduct given;

Reference yield:

7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone (138407-83-7,138512-18-2) → (2'R,3'R,4'S,5'R,6'R)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone (138407-78-0,138512-04-6) + (2'S,3'R,4'S,5'R,6'R)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone (138407-78-0,138512-04-6) + (2'S,3'S,4'S,5'R,6'R)-7-O-<2'-(4',5'-dihydroxy-3'-iodo-6'-phenyltetrahydropyranosyl)>daunomycinone (138512-04-6)

Guidance literature:

With pyridine; hydrogen fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 9h; Yield given. Yields of byproduct given;

upstream raw materials:

7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone

7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone

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