cis-4-methylcyclohexanol p-nitrobenzoate

Base Information

• Chemical Name: cis-4-methylcyclohexanol p-nitrobenzoate
• CAS No.: 75350-73-1
• Molecular Formula: C₁₄H₁₇NO₄
• Molecular Weight: 263.293
• Mol file: 75350-73-1.mol

Synonyms:cis-4-methylcyclohexanol p-nitrobenzoate

Chemical Property of cis-4-methylcyclohexanol p-nitrobenzoate

Chemical Property:

Purity/Quality:

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Technology Process of cis-4-methylcyclohexanol p-nitrobenzoate

There total 1 articles about cis-4-methylcyclohexanol p-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-4-methylcyclohexanol (7731-28-4) → cis-4-methylcyclohexanol p-nitrobenzoate (75350-73-1)

Guidance literature:

DOI:10.2165/00044011-200121120-00004

Reference yield:

cis-4-methylcyclohexanol p-nitrobenzoate (75350-73-1) → 4-methyl-3-cyclohexenol p-nitrobenzoate (75350-77-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / F₂, N₂ / CHCl₃; CCl₃F / -70 °C

2: 70 percent / BF₃*OEt₂

With boron trifluoride diethyl etherate; fluorine; In chloroform; trichlorofluoromethane;

DOI:10.1021/ja00542a039

upstream raw materials:

cis-4-methylcyclohexanol

Downstream raw materials:

4-methyl-3-cyclohexenol p-nitrobenzoate