1,3-bis[2,6-diisopropylphenyl]-4-tert-butyl-4,5-dihydroimidazolinium chloride

Base Information

Chemical Name:1,3-bis[2,6-diisopropylphenyl]-4-tert-butyl-4,5-dihydroimidazolinium chloride
CAS No.:1448990-85-9
Molecular Formula:C₃₁H₄₇N₂*Cl
Molecular Weight:483.181
Hs Code.:

Synonyms:1,3-bis[2,6-diisopropylphenyl]-4-tert-butyl-4,5-dihydroimidazolinium chloride

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Chemical Property of 1,3-bis[2,6-diisopropylphenyl]-4-tert-butyl-4,5-dihydroimidazolinium chloride

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Technology Process of 1,3-bis[2,6-diisopropylphenyl]-4-tert-butyl-4,5-dihydroimidazolinium chloride

There total 4 articles about 1,3-bis[2,6-diisopropylphenyl]-4-tert-butyl-4,5-dihydroimidazolinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1448990-84-8
1-(tert-butyl)-1,2-bis{[2,6-diisopropylphenyl]amino}ethane

: 122-51-0
orthoformic acid triethyl ester

: 1448990-85-9
1,3-bis[2,6-diisopropylphenyl]-4-tert-butyl-4,5-dihydroimidazolinium chloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 130 ℃; for 18h;
DOI:10.1016/j.tetlet.2013.06.132

Reference yield:

: 74663-75-5,134750-23-5
1,2-bis(2,6-diisopropylphenylimino)ethane

: 1448990-85-9
1,3-bis[2,6-diisopropylphenyl]-4-tert-butyl-4,5-dihydroimidazolinium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; diethyl ether / 1 h / 0 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 18 h / 0 - 70 °C

3: hydrogenchloride / 1,4-dioxane / 18 h / 130 °C

With hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; 1,4-dioxane; diethyl ether;
DOI:10.1016/j.tetlet.2013.06.132

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1448990-85-9
1,3-bis[2,6-diisopropylphenyl]-4-tert-butyl-4,5-dihydroimidazolinium chloride

Guidance literature:: Multi-step reaction with 4 steps

1: propan-1-ol; water / 20 h / 20 - 60 °C

2: tetrahydrofuran; diethyl ether / 1 h / 0 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 18 h / 0 - 70 °C

4: hydrogenchloride / 1,4-dioxane / 18 h / 130 °C

With hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; 1,4-dioxane; propan-1-ol; diethyl ether; water;
DOI:10.1016/j.tetlet.2013.06.132