(4S,5R)-3-benzyl 4-methyl 5-methyl-1,2,3-oxathiazolidine-3,4-dicarboxylate 2,2-dioxide

Base Information

Chemical Name:(4S,5R)-3-benzyl 4-methyl 5-methyl-1,2,3-oxathiazolidine-3,4-dicarboxylate 2,2-dioxide
CAS No.:1224632-39-6
Molecular Formula:C₁₃H₁₅NO₇S
Molecular Weight:329.331
Hs Code.:

Synonyms:(4S,5R)-3-benzyl 4-methyl 5-methyl-1,2,3-oxathiazolidine-3,4-dicarboxylate 2,2-dioxide

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Chemical Property of (4S,5R)-3-benzyl 4-methyl 5-methyl-1,2,3-oxathiazolidine-3,4-dicarboxylate 2,2-dioxide

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Technology Process of (4S,5R)-3-benzyl 4-methyl 5-methyl-1,2,3-oxathiazolidine-3,4-dicarboxylate 2,2-dioxide

There total 2 articles about (4S,5R)-3-benzyl 4-methyl 5-methyl-1,2,3-oxathiazolidine-3,4-dicarboxylate 2,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 57224-63-2
methyl (2S,3R)-2-(benzyloxycarbonylamino)-3-hydroxybutyrate

: 1224632-39-6
(4S,5R)-3-benzyl 4-methyl 5-methyl-1,2,3-oxathiazolidine-3,4-dicarboxylate 2,2-dioxide

Guidance literature:: methyl (2S,3R)-2-(benzyloxycarbonylamino)-3-hydroxybutyrate; With pyridine; thionyl chloride; In acetonitrile; at -40 - 20 ℃; Inert atmosphere;

With ruthenium trichloride; sodium periodate; In acetonitrile; Cooling with ice;
DOI:10.1039/c2cc32894a

Reference yield:

: C₁₃H₁₅NO₆S

: 1224632-39-6
(4S,5R)-3-benzyl 4-methyl 5-methyl-1,2,3-oxathiazolidine-3,4-dicarboxylate 2,2-dioxide

Guidance literature:: With ruthenium trichloride; sodium periodate; In water; acetonitrile; at 0 ℃; for 2h;
DOI:10.1021/jo1001388

Reference yield: 93.0%

: 1224632-39-6
(4S,5R)-3-benzyl 4-methyl 5-methyl-1,2,3-oxathiazolidine-3,4-dicarboxylate 2,2-dioxide

: 1224632-46-5
C₂₆H₃₂N₂O₈Se₂

Guidance literature:: (4S,5R)-3-benzyl 4-methyl 5-methyl-1,2,3-oxathiazolidine-3,4-dicarboxylate 2,2-dioxide; With potassium selenocyanate; In acetone; for 5h; Reflux;

With benzyltrimethylammonium tetrathiomolybdate; In acetone; acetonitrile; at 20 ℃; for 8h;

With hydrogenchloride; water; In acetone; acetonitrile; at 20 ℃; for 12h; regioselective reaction;
DOI:10.1021/jo1001388